^(15)N Nuclear Magnetic Resonance Spectroscopy. Natural Abundance^(15)N NMR of Monosubstituted Indoles
Publication type: Journal Article
Publication date: 1976-03-01
scimago Q3
wos Q3
SJR: 0.360
CiteScore: 4.1
Impact factor: 1.4
ISSN: 07491581, 1097458X
General Chemistry
General Materials Science
Abstract
^(15)N chemical shifts of twenty-four substituted indoles have been determined in natural abundance (in organic solvents) using Fourier transform NMR. The overall chemical shift range is 27 ppm, with groups in the 2-, 3- and 5-ring positions showing the largest substituent effects. Substituents capable of resonance interaction with the indole nitrogen give shifts in the expected directions but they cannot be correlated with known substituent parameters. Compounds measured in DMSO give 0·2 to 10·2 ppm downfield shifts with respect to the same compound measured in CDCl_3. ^(13)C NMR data for previously unreported compounds are also reported.
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ROSENBERG E., Williamson K. L., Roberts J. P. ^(15)N Nuclear Magnetic Resonance Spectroscopy. Natural Abundance^(15)N NMR of Monosubstituted Indoles // Magnetic Resonance in Chemistry. 1976. Vol. 8. No. 3. pp. 117-119.
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ROSENBERG E., Williamson K. L., Roberts J. P. ^(15)N Nuclear Magnetic Resonance Spectroscopy. Natural Abundance^(15)N NMR of Monosubstituted Indoles // Magnetic Resonance in Chemistry. 1976. Vol. 8. No. 3. pp. 117-119.
Cite this
RIS
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TY - JOUR
DO - 10.1002/mrc.1270080302
UR - https://doi.org/10.1002/mrc.1270080302
TI - ^(15)N Nuclear Magnetic Resonance Spectroscopy. Natural Abundance^(15)N NMR of Monosubstituted Indoles
T2 - Magnetic Resonance in Chemistry
AU - ROSENBERG, E
AU - Williamson, Kenneth L
AU - Roberts, John Paul
PY - 1976
DA - 1976/03/01
PB - Wiley
SP - 117-119
IS - 3
VL - 8
SN - 0749-1581
SN - 1097-458X
ER -
Cite this
BibTex (up to 50 authors)
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@article{1976_ROSENBERG,
author = {E ROSENBERG and Kenneth L Williamson and John Paul Roberts},
title = {^(15)N Nuclear Magnetic Resonance Spectroscopy. Natural Abundance^(15)N NMR of Monosubstituted Indoles},
journal = {Magnetic Resonance in Chemistry},
year = {1976},
volume = {8},
publisher = {Wiley},
month = {mar},
url = {https://doi.org/10.1002/mrc.1270080302},
number = {3},
pages = {117--119},
doi = {10.1002/mrc.1270080302}
}
Cite this
MLA
Copy
ROSENBERG, E., et al. “^(15)N Nuclear Magnetic Resonance Spectroscopy. Natural Abundance^(15)N NMR of Monosubstituted Indoles.” Magnetic Resonance in Chemistry, vol. 8, no. 3, Mar. 1976, pp. 117-119. https://doi.org/10.1002/mrc.1270080302.