European Polymer Journal, volume 84, pages 205-217
Low-melting phthalonitrile thermosetting monomers with siloxane- and phosphate bridges
Bulgakov Boris
1
,
Babkin Alexander
1
,
Bogolyubov A A
2
,
Sulimov A V
3
,
Kepman A.V.
1
,
Kolyagin Yuri G
1
,
Guseva D. V.
4
,
Rudyak Vladimir
4
,
2
Institute of New Carbon Materials and Technology (INCMaT), 119991, Leninskie Gory, 1-11, Moscow, Russia
|
Publication type: Journal Article
Publication date: 2016-11-01
Journal:
European Polymer Journal
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 6
ISSN: 00143057
Materials Chemistry
Organic Chemistry
General Physics and Astronomy
Polymers and Plastics
Abstract
Abstract The series of low-melting siloxane- and phosphate-bridged phthalonitriles are studied. The monomers of this type possess glass transition temperatures more than 100 °C lower than for common phthalonitriles. Based on the collected experimental data molecular dynamics simulations aimed to predict glass-transition temperatures of the considered types of low-melting phthalonitriles are reported. The validity of computational model is confirmed by successful synthesis of the new monomers, e.g. phosphate- and phosphonate-bridged phthalonitriles are introduced for a first time. Cured Bis(3-(3,4-dicyanophenoxy)phenyl) phenyl phosphate demonstrates thermal performance featured to phthalonitriles (HDT ∼ 450 °C, T 5% = 524 °C, Y c , (Ar) = 80%) along with increased thermo-oxidative stability. In aggregate with convenient processing the considered phthalonitriles can be used as high-temperature matrices for fiber-reinforced plastics production by vacuum infusion or RTM techniques.
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Bulgakov B. et al. Low-melting phthalonitrile thermosetting monomers with siloxane- and phosphate bridges // European Polymer Journal. 2016. Vol. 84. pp. 205-217.
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Bulgakov B., Babkin A., Dzhevakov P. B., Bogolyubov A. A., Sulimov A. V., Kepman A., Kolyagin Y. G., Guseva D. V., Rudyak V., Chertovich A. V. Low-melting phthalonitrile thermosetting monomers with siloxane- and phosphate bridges // European Polymer Journal. 2016. Vol. 84. pp. 205-217.
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TY - JOUR
DO - 10.1016/j.eurpolymj.2016.09.013
UR - https://doi.org/10.1016%2Fj.eurpolymj.2016.09.013
TI - Low-melting phthalonitrile thermosetting monomers with siloxane- and phosphate bridges
T2 - European Polymer Journal
AU - Sulimov, A V
AU - Kepman, A.V.
AU - Bulgakov, Boris
AU - Babkin, Alexander
AU - Dzhevakov, Pavel B
AU - Bogolyubov, A A
AU - Kolyagin, Yuri G
AU - Guseva, D. V.
AU - Rudyak, Vladimir
AU - Chertovich, Alexander V.
PY - 2016
DA - 2016/11/01 00:00:00
PB - Elsevier
SP - 205-217
VL - 84
SN - 0014-3057
ER -
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@article{2016_Bulgakov
author = {A V Sulimov and A.V. Kepman and Boris Bulgakov and Alexander Babkin and Pavel B Dzhevakov and A A Bogolyubov and Yuri G Kolyagin and D. V. Guseva and Vladimir Rudyak and Alexander V. Chertovich},
title = {Low-melting phthalonitrile thermosetting monomers with siloxane- and phosphate bridges},
journal = {European Polymer Journal},
year = {2016},
volume = {84},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016%2Fj.eurpolymj.2016.09.013},
pages = {205--217},
doi = {10.1016/j.eurpolymj.2016.09.013}
}