Food Chemistry, volume 188, pages 51-56
Determination of the total content of some sulfonamides in milk using solid-phase extraction coupled with off-line derivatization and spectrophotometric detection
Publication type: Journal Article
Publication date: 2015-12-01
Journal:
Food Chemistry
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 8.8
ISSN: 03088146, 18737072
General Medicine
Analytical Chemistry
Food Science
Abstract
A simple screening method for isolation and determination of the total content of some sulfonamides in milk using solid-phase extraction and a color reaction is described. This procedure is based on SPE of sulfonamides on hypercrosslinked polystyrene, elution with acetonitrile and off-line derivatization with p-dimethylaminocinnamaldehyde in acetonitrile followed by spectrophotometric determination. The reaction produces intense violet-red color and can be easily used both for quantitation of sulfonamides using spectrophotometry and for naked-eye semi-quantitative estimation. Maximum absorption of the reaction product was determined at 540 nm. The Lambert-Beer's law was obeyed in the range of 0.07-3.0 μg mL(-1) in eluate, with the squared correlation coefficient (R(2)) of 0.9875-0.9995, and the relative standard deviation (RSD) of 3-4%. The limits of SAs detection using preconcentration were of 0.02-0.03 μg mL(-1). The proposed method can be recommended as a routine screening method for quantitation of sulfonamides in milk.
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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1 publication, 1.75%
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Citations by publishers
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5
10
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25
30
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Elsevier
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27 publications, 47.37%
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7 publications, 12.28%
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Wiley
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6 publications, 10.53%
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Multidisciplinary Digital Publishing Institute (MDPI)
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4 publications, 7.02%
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Springer Nature
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4 publications, 7.02%
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American Chemical Society (ACS)
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3 publications, 5.26%
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Pleiades Publishing
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Pleiades Publishing
2 publications, 3.51%
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Zhongguo Kexueyan Ganguang Huaxue Yanjiusuo
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Zhongguo Kexueyan Ganguang Huaxue Yanjiusuo, 1, 1.75%
Zhongguo Kexueyan Ganguang Huaxue Yanjiusuo
1 publication, 1.75%
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Hindawi Limited
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Hindawi Limited
1 publication, 1.75%
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Frontiers Media S.A.
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Frontiers Media S.A.
1 publication, 1.75%
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Dmitrienko S. et al. Determination of the total content of some sulfonamides in milk using solid-phase extraction coupled with off-line derivatization and spectrophotometric detection // Food Chemistry. 2015. Vol. 188. pp. 51-56.
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Dmitrienko S., Kochuk E. V., Tolmacheva V. V., Apyari V., Zolotov Y. A. Determination of the total content of some sulfonamides in milk using solid-phase extraction coupled with off-line derivatization and spectrophotometric detection // Food Chemistry. 2015. Vol. 188. pp. 51-56.
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TY - JOUR
DO - 10.1016/j.foodchem.2015.04.123
UR - https://doi.org/10.1016%2Fj.foodchem.2015.04.123
TI - Determination of the total content of some sulfonamides in milk using solid-phase extraction coupled with off-line derivatization and spectrophotometric detection
T2 - Food Chemistry
AU - Dmitrienko, S
AU - Kochuk, Elena V
AU - Tolmacheva, Veronika V.
AU - Zolotov, Yury A
AU - Apyari, Vladimir
PY - 2015
DA - 2015/12/01 00:00:00
PB - Elsevier
SP - 51-56
VL - 188
SN - 0308-8146
SN - 1873-7072
ER -
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@article{2015_Dmitrienko,
author = {S Dmitrienko and Elena V Kochuk and Veronika V. Tolmacheva and Yury A Zolotov and Vladimir Apyari},
title = {Determination of the total content of some sulfonamides in milk using solid-phase extraction coupled with off-line derivatization and spectrophotometric detection},
journal = {Food Chemistry},
year = {2015},
volume = {188},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016%2Fj.foodchem.2015.04.123},
pages = {51--56},
doi = {10.1016/j.foodchem.2015.04.123}
}