Inorganica Chimica Acta, volume 362, issue 6, pages 1943-1951
Synthesis of palladium(II) 3d-metal(II) paddlewheel acetate-bridged heterodimetallic complexes: Unexpected catalysis by water molecules
Akhmadullina N.S.
1
,
Kozitsyna Natalia Yu.
1
,
Stolarov Igor
1
,
Perova Elena V
1
,
Nefedov Sergei E
1
,
Publication type: Journal Article
Publication date: 2009-04-01
Journal:
Inorganica Chimica Acta
Quartile SCImago
Q2
Quartile WOS
Q2
Impact factor: 2.8
ISSN: 00201693, 18733255
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The reaction of Pd 3 (μ-OOCMe) 6 ( 1 ) with 3d-metal acetates (Ni II , Co II , Cu II ) in acetic acid is triggered by the primary hydrolytic cleavage of an acetate bridge in molecule 1 , affording 1D polymeric complexes {Pd(μ-OOCMe) 4 M(OH 2 )(HOOCMe) 2 } n built of the paddlewheel units [Pd(μ-OOCMe) 4 M] linked trough the H-bonded H 2 O and MeCOOH molecules. A study of the reaction kinetics between the trinuclear palladium(II) acetate Pd 3 (μ-OOCMe) 6 ( 1 ) and the mononuclear 3d-metal (Ni II , Co II , Cu II ) acetates in acetic acid under water-specified conditions revealed a fairly complicated reaction mechanism triggered by the primary hydrolytic cleavage of an acetate bridge in molecule 1 . The isolated reaction products, as established by X-ray diffraction study, are 1D polymeric complexes {Pd(μ-OOCMe) 4 M(OH 2 )(HOOCMe) 2 } n (M = Ni II , Co II , Cu II , Mn II , Zn II ) built of the Pd II -based paddlewheel units [Pd(μ-OOCMe) 4 M] and linked trough the H-bonded H 2 O and MeCOOH molecules.
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Akhmadullina N. et al. Synthesis of palladium(II) 3d-metal(II) paddlewheel acetate-bridged heterodimetallic complexes: Unexpected catalysis by water molecules // Inorganica Chimica Acta. 2009. Vol. 362. No. 6. pp. 1943-1951.
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Akhmadullina N., Cherkashina N. V., Kozitsyna N. Y., Stolarov I., Perova E. V., Gekhman A. E., Nefedov S. E., Vargaftik M., Moiseev I. I. Synthesis of palladium(II) 3d-metal(II) paddlewheel acetate-bridged heterodimetallic complexes: Unexpected catalysis by water molecules // Inorganica Chimica Acta. 2009. Vol. 362. No. 6. pp. 1943-1951.
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TY - JOUR
DO - 10.1016/j.ica.2008.09.042
UR - https://doi.org/10.1016%2Fj.ica.2008.09.042
TI - Synthesis of palladium(II) 3d-metal(II) paddlewheel acetate-bridged heterodimetallic complexes: Unexpected catalysis by water molecules
T2 - Inorganica Chimica Acta
AU - Akhmadullina, N.S.
AU - Cherkashina, Natalia V.
AU - Kozitsyna, Natalia Yu.
AU - Stolarov, Igor
AU - Perova, Elena V
AU - Gekhman, Alexander E.
AU - Nefedov, Sergei E
AU - Vargaftik, Michael
AU - Moiseev, I. I.
PY - 2009
DA - 2009/04/01 00:00:00
PB - Elsevier
SP - 1943-1951
IS - 6
VL - 362
SN - 0020-1693
SN - 1873-3255
ER -
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@article{2009_Akhmadullina,
author = {N.S. Akhmadullina and Natalia V. Cherkashina and Natalia Yu. Kozitsyna and Igor Stolarov and Elena V Perova and Alexander E. Gekhman and Sergei E Nefedov and Michael Vargaftik and I. I. Moiseev},
title = {Synthesis of palladium(II) 3d-metal(II) paddlewheel acetate-bridged heterodimetallic complexes: Unexpected catalysis by water molecules},
journal = {Inorganica Chimica Acta},
year = {2009},
volume = {362},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016%2Fj.ica.2008.09.042},
number = {6},
pages = {1943--1951},
doi = {10.1016/j.ica.2008.09.042}
}
Cite this
MLA
Copy
Akhmadullina, N.S., et al. “Synthesis of palladium(II) 3d-metal(II) paddlewheel acetate-bridged heterodimetallic complexes: Unexpected catalysis by water molecules.” Inorganica Chimica Acta, vol. 362, no. 6, Apr. 2009, pp. 1943-1951. https://doi.org/10.1016%2Fj.ica.2008.09.042.