Novel 1D coordination polymer {Tm(Piv)3}n: Synthesis, structure, magnetic properties and thermal behavior
Irina Fomina
1
,
Mikhail Bykov
2
,
Irina Malkerova
1
,
Zhanna Dobrokhotova
1
,
Grygory Aleksandrov
1
,
Anna Emelina
2
,
Lada Puntus
3
,
Vladimir Novotortsev
1
,
Publication type: Journal Article
Publication date: 2012-01-01
scimago Q2
wos Q1
SJR: 0.629
CiteScore: 6.8
Impact factor: 3.5
ISSN: 00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
Abstract The new 1D coordination polymer {Tm(Piv)3}n (1), where Piv=OOCBut−, was synthesized in high yield (>95%) by the reaction of thulium acetate with pivalic acid in air at 100 °С. According to the X-ray diffraction data, the metal atoms in compound 1 are in an octahedral ligand environment unusual for lanthanides. The magnetic and luminescence properties of polymer 1, it’s the solid-phase thermal decomposition in air and under argon, and the thermal behavior in the temperature range of −50…+50 °С were investigated. The vaporization process of complex 1 was studied by the Knudsen effusion method combined with mass-spectrometric analysis of the gas-phase composition in the temperature range of 570–680 K.
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Bykov M. et al. Novel 1D coordination polymer {Tm(Piv)3}n: Synthesis, structure, magnetic properties and thermal behavior // Journal of Solid State Chemistry. 2012. Vol. 185. pp. 49-55.
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Fomina I., Bykov M., Malkerova I., Dobrokhotova Z., Aleksandrov G., Emelina A., Puntus L., Novotortsev V., Bogomyakov A. S., Eremenko I. L. Novel 1D coordination polymer {Tm(Piv)3}n: Synthesis, structure, magnetic properties and thermal behavior // Journal of Solid State Chemistry. 2012. Vol. 185. pp. 49-55.
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TY - JOUR
DO - 10.1016/j.jssc.2011.09.033
UR - https://doi.org/10.1016/j.jssc.2011.09.033
TI - Novel 1D coordination polymer {Tm(Piv)3}n: Synthesis, structure, magnetic properties and thermal behavior
T2 - Journal of Solid State Chemistry
AU - Fomina, Irina
AU - Bykov, Mikhail
AU - Malkerova, Irina
AU - Dobrokhotova, Zhanna
AU - Aleksandrov, Grygory
AU - Emelina, Anna
AU - Puntus, Lada
AU - Novotortsev, Vladimir
AU - Bogomyakov, Artem S
AU - Eremenko, Igor L.
PY - 2012
DA - 2012/01/01
PB - Elsevier
SP - 49-55
VL - 185
SN - 0022-4596
SN - 1095-726X
ER -
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BibTex (up to 50 authors)
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@article{2012_Bykov,
author = {Irina Fomina and Mikhail Bykov and Irina Malkerova and Zhanna Dobrokhotova and Grygory Aleksandrov and Anna Emelina and Lada Puntus and Vladimir Novotortsev and Artem S Bogomyakov and Igor L. Eremenko},
title = {Novel 1D coordination polymer {Tm(Piv)3}n: Synthesis, structure, magnetic properties and thermal behavior},
journal = {Journal of Solid State Chemistry},
year = {2012},
volume = {185},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/j.jssc.2011.09.033},
pages = {49--55},
doi = {10.1016/j.jssc.2011.09.033}
}