Synthesis, self-assembly and the effect of the macrocyclic platform on thermal properties of lactic acid oligomer modified by p-tert-butylthiacalix[4]arene
Publication type: Journal Article
Publication date: 2019-05-01
scimago Q1
wos Q1
SJR: 0.935
CiteScore: 10.5
Impact factor: 5.2
ISSN: 01677322, 18733166
Materials Chemistry
Electronic, Optical and Magnetic Materials
Physical and Theoretical Chemistry
Spectroscopy
Atomic and Molecular Physics, and Optics
Condensed Matter Physics
Abstract
The interaction of (L)-lactic acid with p-tert-butylthiacalix[4]arene containing ethoxycarbonyl fragments in the 1,3-alternate conformation was studied in tetraglyme. For the first time, the lactic acid oligomer was obtained by polycondensation with the macrocycle and characterized by 1H, 13C NMR, IR spectroscopy, MALDI mass spectrometry and gel permeation chromatography. Thermal stability of the obtained copolyester of lactic acid and thiacalix[4]arene was studied by TG/DSC analysis and the effect of the macrocyclic platform on its thermal properties was shown. Copolyester obtained was thermally more stable than oligolactic acid. Self-assembly of synthesized oligomer was studied by dynamic light scattering method. It was shown that monodisperse particles (PDI = 0.13) with the size of 208 ± 4 nm are formed in CH3CN solution at 2.5 × 10−5 M concentration.
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Vavilova A. A. et al. Synthesis, self-assembly and the effect of the macrocyclic platform on thermal properties of lactic acid oligomer modified by p-tert-butylthiacalix[4]arene // Journal of Molecular Liquids. 2019. Vol. 281. pp. 243-251.
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Vavilova A. A., Gorbachuk V. V., Shurpik D. N., Gerasimov A., Yakimova L., Padnya P., Stoikov I. Synthesis, self-assembly and the effect of the macrocyclic platform on thermal properties of lactic acid oligomer modified by p-tert-butylthiacalix[4]arene // Journal of Molecular Liquids. 2019. Vol. 281. pp. 243-251.
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TY - JOUR
DO - 10.1016/j.molliq.2019.02.086
UR - https://doi.org/10.1016/j.molliq.2019.02.086
TI - Synthesis, self-assembly and the effect of the macrocyclic platform on thermal properties of lactic acid oligomer modified by p-tert-butylthiacalix[4]arene
T2 - Journal of Molecular Liquids
AU - Vavilova, Alena A
AU - Gorbachuk, Vladimir V
AU - Shurpik, Dmitriy N
AU - Gerasimov, Alexander
AU - Yakimova, Luidmila
AU - Padnya, Pavel
AU - Stoikov, Ivan
PY - 2019
DA - 2019/05/01
PB - Elsevier
SP - 243-251
VL - 281
SN - 0167-7322
SN - 1873-3166
ER -
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@article{2019_Vavilova,
author = {Alena A Vavilova and Vladimir V Gorbachuk and Dmitriy N Shurpik and Alexander Gerasimov and Luidmila Yakimova and Pavel Padnya and Ivan Stoikov},
title = {Synthesis, self-assembly and the effect of the macrocyclic platform on thermal properties of lactic acid oligomer modified by p-tert-butylthiacalix[4]arene},
journal = {Journal of Molecular Liquids},
year = {2019},
volume = {281},
publisher = {Elsevier},
month = {may},
url = {https://doi.org/10.1016/j.molliq.2019.02.086},
pages = {243--251},
doi = {10.1016/j.molliq.2019.02.086}
}