Journal of Molecular Structure, volume 1251, pages 132066

Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts

Publication typeJournal Article
Publication date2022-03-01
Quartile SCImago
Q2
Quartile WOS
Q2
Impact factor3.8
ISSN00222860
Organic Chemistry
Inorganic Chemistry
Spectroscopy
Analytical Chemistry
Abstract
• Six ferrocene-based phenylethylamino compounds as burning rate catalysts were prepared. • Effect of burning rate catalysts on thermal decomposition of ammonium perchlorate was investigated. • Anti-migration behavior of catalysts in simulated propellant was investigated. • Catalytic mechanism on thermal decomposition of ammonium perchlorate and anti-migration mechanism of catalysts in simulated propellant were studied. • Decomposition temperature of ammonium perchlorate was decreased and the anti-migration ability of catalysts was improved significantly. Ferrocene (Fc)-based compounds as common burning rate catalysts (BRCs) are often used in composite solid propellants, such as catocene ( Cat ). To solve the migration problem of common Fc-based compounds, six novel ferrocene (Fc)-based phenylethylamino BRCs were designed and synthesized. Their structures as well as catalytic performance for ammonium perchlorate (AP) decomposition were studied by UV–Vis, FT-IR, 1 H NMR, 19 F NMR, ESI-MS, EA, CV and TG, respectively. The test results indicated that these Fc-based phenylethylamino BRCs had good catalytic activity for thermal decomposition of AP and better anti-migration ability than Cat and Fc in simulated AP-based propellant. Among these compounds, Fc-2 showed the best catalytic activity for thermal decomposition of AP and Fc-6 showed the best anti-migration ability. This study demonstrates that Fc-based phenylethylamino compounds are promising BRCs for AP-based propellant.

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GOST Copy
Wang L. et al. Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts // Journal of Molecular Structure. 2022. Vol. 1251. p. 132066.
GOST all authors (up to 50) Copy
Wang L., Huang Z., Amin B. U., Liu J., Yu H., Wang L., Vatsadze S. Z. Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts // Journal of Molecular Structure. 2022. Vol. 1251. p. 132066.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.molstruc.2021.132066
UR - https://doi.org/10.1016%2Fj.molstruc.2021.132066
TI - Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts
T2 - Journal of Molecular Structure
AU - Wang, Li
AU - Huang, Zhikun
AU - Amin, Bilal Ul
AU - Liu, Jinyi
AU - Yu, Haojie
AU - Wang, Li
AU - Vatsadze, Sergey Z.
PY - 2022
DA - 2022/03/01 00:00:00
PB - Elsevier
SP - 132066
VL - 1251
SN - 0022-2860
ER -
BibTex
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BibTex Copy
@article{2022_Wang
author = {Li Wang and Zhikun Huang and Bilal Ul Amin and Jinyi Liu and Haojie Yu and Li Wang and Sergey Z. Vatsadze},
title = {Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts},
journal = {Journal of Molecular Structure},
year = {2022},
volume = {1251},
publisher = {Elsevier},
month = {mar},
url = {https://doi.org/10.1016%2Fj.molstruc.2021.132066},
pages = {132066},
doi = {10.1016/j.molstruc.2021.132066}
}
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