Journal of Molecular Structure, volume 1251, pages 132066
Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts
Publication type: Journal Article
Publication date: 2022-03-01
Journal:
Journal of Molecular Structure
Quartile SCImago
Q2
Quartile WOS
Q2
Impact factor: 3.8
ISSN: 00222860
Organic Chemistry
Inorganic Chemistry
Spectroscopy
Analytical Chemistry
Abstract
• Six ferrocene-based phenylethylamino compounds as burning rate catalysts were prepared. • Effect of burning rate catalysts on thermal decomposition of ammonium perchlorate was investigated. • Anti-migration behavior of catalysts in simulated propellant was investigated. • Catalytic mechanism on thermal decomposition of ammonium perchlorate and anti-migration mechanism of catalysts in simulated propellant were studied. • Decomposition temperature of ammonium perchlorate was decreased and the anti-migration ability of catalysts was improved significantly. Ferrocene (Fc)-based compounds as common burning rate catalysts (BRCs) are often used in composite solid propellants, such as catocene ( Cat ). To solve the migration problem of common Fc-based compounds, six novel ferrocene (Fc)-based phenylethylamino BRCs were designed and synthesized. Their structures as well as catalytic performance for ammonium perchlorate (AP) decomposition were studied by UV–Vis, FT-IR, 1 H NMR, 19 F NMR, ESI-MS, EA, CV and TG, respectively. The test results indicated that these Fc-based phenylethylamino BRCs had good catalytic activity for thermal decomposition of AP and better anti-migration ability than Cat and Fc in simulated AP-based propellant. Among these compounds, Fc-2 showed the best catalytic activity for thermal decomposition of AP and Fc-6 showed the best anti-migration ability. This study demonstrates that Fc-based phenylethylamino compounds are promising BRCs for AP-based propellant.
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Wang L. et al. Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts // Journal of Molecular Structure. 2022. Vol. 1251. p. 132066.
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Wang L., Huang Z., Amin B. U., Liu J., Yu H., Wang L., Vatsadze S. Z. Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts // Journal of Molecular Structure. 2022. Vol. 1251. p. 132066.
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TY - JOUR
DO - 10.1016/j.molstruc.2021.132066
UR - https://doi.org/10.1016%2Fj.molstruc.2021.132066
TI - Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts
T2 - Journal of Molecular Structure
AU - Wang, Li
AU - Huang, Zhikun
AU - Amin, Bilal Ul
AU - Liu, Jinyi
AU - Yu, Haojie
AU - Wang, Li
AU - Vatsadze, Sergey Z.
PY - 2022
DA - 2022/03/01 00:00:00
PB - Elsevier
SP - 132066
VL - 1251
SN - 0022-2860
ER -
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@article{2022_Wang
author = {Li Wang and Zhikun Huang and Bilal Ul Amin and Jinyi Liu and Haojie Yu and Li Wang and Sergey Z. Vatsadze},
title = {Preparation of ferrocene-based phenylethylamino compounds and their properties as burning rate catalysts},
journal = {Journal of Molecular Structure},
year = {2022},
volume = {1251},
publisher = {Elsevier},
month = {mar},
url = {https://doi.org/10.1016%2Fj.molstruc.2021.132066},
pages = {132066},
doi = {10.1016/j.molstruc.2021.132066}
}
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