Synthesis, structure and thermolysis of Ba(II)–M(II) (M = Co, Zn) bimetallic 3D-polymers as precursors of complex oxides
Mikhail A Ryumin
1
,
Zhanna V Dobrokhotova
1
,
Anna L Emelina
2
,
Mikhail A Bukov
2
,
K. S. Gavrichev
1
,
A.V Sidorov
1
,
Igor L. Eremenko
1
,
Vladimir M. Novotortsev
1
Publication type: Journal Article
Publication date: 2015-02-01
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract The Ba–Co and Ba–Zn heterometallic 3D-polymers [BaM(H2O)5(Me2mal)2]n, where Me2mal2− is the dimethylmalonic acid dianion, MII = Co (1), Zn (2), were synthesized by the reactions of CoSO4 or Zn(OAc)2, respectively, with Ba(OH)2 in water. The thermal dehydration of 1 and 2 occurs in one step. A kinetic model for the dehydration of complexes 1 and 2 is proposed. Crystalline BaCoO3−x and BaZnO2 were formed as a result of solid state thermolysis of 1 and 2 under the following conditions: air flow rate 60 ml/min, heating rate 10 °C/min up to t = 800 °C (1) or 750 °C (2), followed by storage for 12 h at the same temperatures.
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Total citations:
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Ryumin M. A. et al. Synthesis, structure and thermolysis of Ba(II)–M(II) (M = Co, Zn) bimetallic 3D-polymers as precursors of complex oxides // Polyhedron. 2015. Vol. 87. pp. 28-37.
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Ryumin M. A., Dobrokhotova Z. V., Emelina A. L., Bukov M. A., Gogoleva N. V., Gavrichev K. S., Zorina-Tikhonova E. N., Demina L. I., Kiskin M. A., Sidorov A., Eremenko I. L., Novotortsev V. M. Synthesis, structure and thermolysis of Ba(II)–M(II) (M = Co, Zn) bimetallic 3D-polymers as precursors of complex oxides // Polyhedron. 2015. Vol. 87. pp. 28-37.
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TY - JOUR
DO - 10.1016/j.poly.2014.10.031
UR - https://doi.org/10.1016/j.poly.2014.10.031
TI - Synthesis, structure and thermolysis of Ba(II)–M(II) (M = Co, Zn) bimetallic 3D-polymers as precursors of complex oxides
T2 - Polyhedron
AU - Ryumin, Mikhail A
AU - Dobrokhotova, Zhanna V
AU - Emelina, Anna L
AU - Bukov, Mikhail A
AU - Gogoleva, Natalya V
AU - Gavrichev, K. S.
AU - Zorina-Tikhonova, Ekaterina N.
AU - Demina, Liudmila I
AU - Kiskin, Mikhail A.
AU - Sidorov, A.V
AU - Eremenko, Igor L.
AU - Novotortsev, Vladimir M.
PY - 2015
DA - 2015/02/01
PB - Elsevier
SP - 28-37
VL - 87
SN - 0277-5387
SN - 1873-3719
ER -
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BibTex (up to 50 authors)
Copy
@article{2015_Ryumin,
author = {Mikhail A Ryumin and Zhanna V Dobrokhotova and Anna L Emelina and Mikhail A Bukov and Natalya V Gogoleva and K. S. Gavrichev and Ekaterina N. Zorina-Tikhonova and Liudmila I Demina and Mikhail A. Kiskin and A.V Sidorov and Igor L. Eremenko and Vladimir M. Novotortsev},
title = {Synthesis, structure and thermolysis of Ba(II)–M(II) (M = Co, Zn) bimetallic 3D-polymers as precursors of complex oxides},
journal = {Polyhedron},
year = {2015},
volume = {87},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/j.poly.2014.10.031},
pages = {28--37},
doi = {10.1016/j.poly.2014.10.031}
}