Synthesis and characterization of new complexes derived from 4-thienyl substituted pyrimidines
Ekaterina M Cheprakova
1, 2
,
Egor V. Verbitskiy
1, 2
,
Grigory G. Aleksandrov
3
,
Yuri N Shvachko
4
,
Igor L. Eremenko
3
,
Gennady L. Rusinov
1, 2
,
Valery Charushin
1, 2
Тип публикации: Journal Article
Дата публикации: 2015-11-01
scimago Q3
wos Q2
БС2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
Abstract The behavior of 4-thienyl substituted pyrimidine ligands (L1–3) has been studied for the series of their reactions with various salts of 3d metals (Co, Zn, Ni, Cu) and platinoids (Pt, Pd). In particular, mononuclear Co(OTf)2(L1–3)2(H2O)2(MeCN)2 (1), binuclear Co2(Piv)2(L1–3)4 (2a,b), Cu2(Piv)2(L1–3)2 (5a,b), heterometallic polynuclear Li2Co2(Piv)6(L1–3)2 (4) and chelate [(L1)Pd(OAc)]2 (6) complexes have been obtained. The structures of all complexes have been established by X-ray diffraction. Also magnetic properties of coordination compounds 1, 2, 4 and 5 have been studied in details. In particular, mononuclear Co(II) complexes 1 and 4 proved to exhibit paramagnetism with large positive zero-field splitting parameters. Dinuclear Co(II) complexes 2a,b show weak antiferromagnetic interactions. Dinuclear Cu(II) complexes 5a,b demonstrate strong antiferromagnetic superexchange interactions via four carboxylate bridges. The systems 2a,b and 5a,b are isolated as exchange coupled dimers.
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Cheprakova E. M. et al. Synthesis and characterization of new complexes derived from 4-thienyl substituted pyrimidines // Polyhedron. 2015. Vol. 100. pp. 89-99.
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Cheprakova E. M., Verbitskiy E. V., Kiskin M. A., Aleksandrov G. G., Slepukhin P. A., Sidorov A. A., Starichenko D., Shvachko Y. N., Eremenko I. L., Rusinov G. L., Charushin V. Synthesis and characterization of new complexes derived from 4-thienyl substituted pyrimidines // Polyhedron. 2015. Vol. 100. pp. 89-99.
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TY - JOUR
DO - 10.1016/j.poly.2015.07.016
UR - https://doi.org/10.1016/j.poly.2015.07.016
TI - Synthesis and characterization of new complexes derived from 4-thienyl substituted pyrimidines
T2 - Polyhedron
AU - Cheprakova, Ekaterina M
AU - Verbitskiy, Egor V.
AU - Kiskin, Mikhail A.
AU - Aleksandrov, Grigory G.
AU - Slepukhin, Pavel A.
AU - Sidorov, Aleksei A.
AU - Starichenko, Denis
AU - Shvachko, Yuri N
AU - Eremenko, Igor L.
AU - Rusinov, Gennady L.
AU - Charushin, Valery
PY - 2015
DA - 2015/11/01
PB - Elsevier
SP - 89-99
VL - 100
SN - 0277-5387
SN - 1873-3719
ER -
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@article{2015_Cheprakova,
author = {Ekaterina M Cheprakova and Egor V. Verbitskiy and Mikhail A. Kiskin and Grigory G. Aleksandrov and Pavel A. Slepukhin and Aleksei A. Sidorov and Denis Starichenko and Yuri N Shvachko and Igor L. Eremenko and Gennady L. Rusinov and Valery Charushin},
title = {Synthesis and characterization of new complexes derived from 4-thienyl substituted pyrimidines},
journal = {Polyhedron},
year = {2015},
volume = {100},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.poly.2015.07.016},
pages = {89--99},
doi = {10.1016/j.poly.2015.07.016}
}