Elsevier
Polyhedron
,  volume 100 ,  pages 344-350

Influence of the rac–meso isomerization of seven-membered cyclic bisphosphines on the predominant formation of chelate complexes

Publication type: Journal Article
Publication date: 2015-11-01
Elsevier
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The seven-membered cyclic bisphosphines 3–5 were synthesized by a Mannich-like condensation reaction of 1,2-bis(phenylphosphino)ethane, formaldehyde and primary amines (tert-butylamine, 1,1-(diphenyl)methylamine, (2R)-tetrahydro-2-furanylmethylamine) as a mixture of RPRP/SPSP (rac, 3a–5a) and RPSP (meso, 3b–5b) stereoisomers. The structures of the rac stereoisomers 3a–5a were investigated by X-ray crystal structure analyses. The RR/SS to RS isomerization of 3–5 and oxidation processes of 4 in solution were studied. Platinum(II) P,P-chelate complexes are formed exclusively from rac/meso mixtures of 3–5.
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GOST Copy
Musina E. et al. Influence of the rac–meso isomerization of seven-membered cyclic bisphosphines on the predominant formation of chelate complexes // Polyhedron. 2015. Vol. 100. pp. 344-350.
GOST all authors (up to 50) Copy
Musina E., Wittmann T. I., Strelnik I. D., Naumova O. E., Karasik A. A., Krivolapov D. B., R. Islamov D., Kataeva O., Sinyashin O. G., Lönnecke P., Hey-Hawkins E. Influence of the rac–meso isomerization of seven-membered cyclic bisphosphines on the predominant formation of chelate complexes // Polyhedron. 2015. Vol. 100. pp. 344-350.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1016/j.poly.2015.08.033
UR - https://linkinghub.elsevier.com/retrieve/pii/S0277538715004799
TI - Influence of the rac–meso isomerization of seven-membered cyclic bisphosphines on the predominant formation of chelate complexes
T2 - Polyhedron
AU - Musina, Elvira
AU - Wittmann, Tatiana I
AU - Strelnik, Igor D
AU - Naumova, Olga E
AU - Karasik, Andrey A
AU - Krivolapov, Dmitry B.
AU - R. Islamov, Daut
AU - Kataeva, O.N.
AU - Sinyashin, Oleg G.
AU - Lönnecke, Peter
AU - Hey-Hawkins, Evamarie
PY - 2015
DA - 2015/11/01
PB - Elsevier
SP - 344-350
VL - 100
SN - 0277-5387
SN - 1873-3719
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2015_Musina,
author = {Elvira Musina and Tatiana I Wittmann and Igor D Strelnik and Olga E Naumova and Andrey A Karasik and Dmitry B. Krivolapov and Daut R. Islamov and O.N. Kataeva and Oleg G. Sinyashin and Peter Lönnecke and Evamarie Hey-Hawkins},
title = {Influence of the rac–meso isomerization of seven-membered cyclic bisphosphines on the predominant formation of chelate complexes},
journal = {Polyhedron},
year = {2015},
volume = {100},
publisher = {Elsevier},
month = {nov},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0277538715004799},
pages = {344--350},
doi = {10.1016/j.poly.2015.08.033}
}