Copper(II) complexes bearing o-iminosemiquinonate ligands with augmented aromatic substituents
Kira I Pashanova
1
,
N. T. Berberova
3
,
Тип публикации: Journal Article
Дата публикации: 2016-11-01
scimago Q3
wos Q2
БС2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
Two tetracoordinated bis- o -iminosemiquinonato complexes, imSQ C(O)Ph 2 Cu ( 1 ) and imSQ Ph 2 Cu ( 2 ), based on the new o -aminophenols H 2 L C(O)Ph and H 2 L Ph , functionalized in the ortho-position of the N-aryl fragment, were synthesized. Compound 1 is square-planar with a weak secondary interaction between the phenyl ring of the C(O)Ph group and copper center, whereas complex 2 is characterized by a distorted planar geometry with cis-positions of the phenyl groups with respect to each other. Compounds 1 and 2 exhibit an S = 1/2 spin ground state with strong antiferromagnetic coupling between the o -iminosemiquinone ligands, as established by variable-temperature magnetic susceptibility measurements. EPR measurements indicated the presence of an unpaired electron at the Cu(II) center in both complexes at low temperature. The electrochemical behavior of 1 and 2 was investigated by cyclic voltammetry.
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Piskunov A. V. et al. Copper(II) complexes bearing o-iminosemiquinonate ligands with augmented aromatic substituents // Polyhedron. 2016. Vol. 119. pp. 286-292.
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Piskunov A. V., Pashanova K. I., Bogomyakov A. S., Smolyaninov I. V., Berberova N. T., Fukin G. K. Copper(II) complexes bearing o-iminosemiquinonate ligands with augmented aromatic substituents // Polyhedron. 2016. Vol. 119. pp. 286-292.
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TY - JOUR
DO - 10.1016/j.poly.2016.08.033
UR - https://doi.org/10.1016/j.poly.2016.08.033
TI - Copper(II) complexes bearing o-iminosemiquinonate ligands with augmented aromatic substituents
T2 - Polyhedron
AU - Piskunov, Alexander V.
AU - Pashanova, Kira I
AU - Bogomyakov, Artem S
AU - Smolyaninov, Ivan V.
AU - Berberova, N. T.
AU - Fukin, Georgy K.
PY - 2016
DA - 2016/11/01
PB - Elsevier
SP - 286-292
VL - 119
SN - 0277-5387
SN - 1873-3719
ER -
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@article{2016_Piskunov,
author = {Alexander V. Piskunov and Kira I Pashanova and Artem S Bogomyakov and Ivan V. Smolyaninov and N. T. Berberova and Georgy K. Fukin},
title = {Copper(II) complexes bearing o-iminosemiquinonate ligands with augmented aromatic substituents},
journal = {Polyhedron},
year = {2016},
volume = {119},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.poly.2016.08.033},
pages = {286--292},
doi = {10.1016/j.poly.2016.08.033}
}