Selective synthesis of the [2-B10H9I]2− anion and some theoretical aspects of its iodination process
Publication type: Journal Article
Publication date: 2018-01-01
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
New approaches to the selective synthesis of the [2-B10H9I]− anion have been reported based on careful control of the reaction medium acidity. The mechanism of the iodination was proposed and the regioselectivity of electrophilic substitution of the [B10H10]2− anion was explained based on B3LYP-calculations of the potential energy surface of the system using the mixed basis 6-31G∗/LanL2DZ. The obtained compounds were characterized by IR and NMR (1H and 11B) spectroscopy, together with ESI-MS-spectrometry. The crystal structures of (PPh4)2[2-B10H9I] and {(PPh4)2[2-B10H9I]·2C4H8O2} were determined by X-ray diffraction.
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Zhdanov A. P. et al. Selective synthesis of the [2-B10H9I]2− anion and some theoretical aspects of its iodination process // Polyhedron. 2018. Vol. 139. pp. 125-130.
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Zhdanov A. P., Zhdanova K. A., Bykov A. Yu., Kochnev V. K., Grigoriev M. S., Zhizhin K. Y., Kuznetsov N. T. Selective synthesis of the [2-B10H9I]2− anion and some theoretical aspects of its iodination process // Polyhedron. 2018. Vol. 139. pp. 125-130.
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TY - JOUR
DO - 10.1016/j.poly.2017.09.050
UR - https://doi.org/10.1016/j.poly.2017.09.050
TI - Selective synthesis of the [2-B10H9I]2− anion and some theoretical aspects of its iodination process
T2 - Polyhedron
AU - Zhdanov, Andrey P.
AU - Zhdanova, K A
AU - Bykov, A Yu
AU - Kochnev, V K
AU - Grigoriev, Mikhail S.
AU - Zhizhin, Konstantin Yu.
AU - Kuznetsov, N. T.
PY - 2018
DA - 2018/01/01
PB - Elsevier
SP - 125-130
VL - 139
SN - 0277-5387
SN - 1873-3719
ER -
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@article{2018_Zhdanov,
author = {Andrey P. Zhdanov and K A Zhdanova and A Yu Bykov and V K Kochnev and Mikhail S. Grigoriev and Konstantin Yu. Zhizhin and N. T. Kuznetsov},
title = {Selective synthesis of the [2-B10H9I]2− anion and some theoretical aspects of its iodination process},
journal = {Polyhedron},
year = {2018},
volume = {139},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/j.poly.2017.09.050},
pages = {125--130},
doi = {10.1016/j.poly.2017.09.050}
}