Reactive and Functional Polymers, volume 139, pages 34-41

Bis(4-cyanophenyl) phenyl phosphate as viscosity reducing comonomer for phthalonitrile resins

Publication type: Journal Article
Publication date: 2019-06-01
Quartile SCImago
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Quartile WOS
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Impact factor: 5.1
ISSN: 13815148
Materials Chemistry
General Chemistry
Biochemistry
General Chemical Engineering
Polymers and Plastics
Environmental Chemistry
Abstract
Abstract Bis(4-cyanophenyl) phenyl phosphate (CPP) is introduced for the first time as a viscosity reducing comonomer for phthalonitrile resins. In comparison to the common phthalonitrile resins, the blends of CPP with 4,4′-[benzene-1,3-diylbis(oxy)]diphthalonitrile demonstrated advanced processing properties suitable for cost-effective injection processing (η as low as to 180 mPa∙s at 100 °C). Thermal copolymerization was performed indicating complete inclusion of bis-benzonitrile CPP into the phthalonitrile network resulting in formation of thermosets with great thermal performance. Hydrolysis of CPP at pH 4, 7, and 10 was studied to confirm its suitability as a reactive diluent for phthalonitrile. Conversion vs. time plots were obtained via HPLC analysis, and pseudo-first order rate constants were determined in the range of 25–80 °C. The activation parameters were calculated from the Arrhenius equation.
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Terekhov V. E. et al. Bis(4-cyanophenyl) phenyl phosphate as viscosity reducing comonomer for phthalonitrile resins // Reactive and Functional Polymers. 2019. Vol. 139. pp. 34-41.
GOST all authors (up to 50) Copy
Terekhov V. E., Aleshkevich V. V., Afanaseva E. S., Nechausov S. S., Babkin A., Bulgakov B. A., Kepman A., Avdeev V. V., Babkin A., Bulgakov B. Bis(4-cyanophenyl) phenyl phosphate as viscosity reducing comonomer for phthalonitrile resins // Reactive and Functional Polymers. 2019. Vol. 139. pp. 34-41.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.reactfunctpolym.2019.03.010
UR - https://doi.org/10.1016%2Fj.reactfunctpolym.2019.03.010
TI - Bis(4-cyanophenyl) phenyl phosphate as viscosity reducing comonomer for phthalonitrile resins
T2 - Reactive and Functional Polymers
AU - Terekhov, V E
AU - Aleshkevich, V V
AU - Afanaseva, E S
AU - Nechausov, S S
AU - Babkin, A.V.
AU - Bulgakov, B A
AU - Kepman, A.V.
AU - Avdeev, V V
AU - Babkin, Alexander
AU - Bulgakov, Boris
PY - 2019
DA - 2019/06/01 00:00:00
PB - Elsevier
SP - 34-41
VL - 139
SN - 1381-5148
ER -
BibTex
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@article{2019_Terekhov,
author = {V E Terekhov and V V Aleshkevich and E S Afanaseva and S S Nechausov and A.V. Babkin and B A Bulgakov and A.V. Kepman and V V Avdeev and Alexander Babkin and Boris Bulgakov},
title = {Bis(4-cyanophenyl) phenyl phosphate as viscosity reducing comonomer for phthalonitrile resins},
journal = {Reactive and Functional Polymers},
year = {2019},
volume = {139},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1016%2Fj.reactfunctpolym.2019.03.010},
pages = {34--41},
doi = {10.1016/j.reactfunctpolym.2019.03.010}
}
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