Talanta, volume 152, pages 203-210

Facile synthesis of magnetic hypercrosslinked polystyrene and its application in the magnetic solid-phase extraction of sulfonamides from water and milk samples before their HPLC determination

Publication typeJournal Article
Publication date2016-05-01
Journal: Talanta
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor6.1
ISSN00399140, 18733573
Analytical Chemistry
Abstract
In this study, a novel magnetic solid-phase extraction (MSPE) sorbent, magnetic hypercrosslinked polystyrene (HCP/Fe3O4), was prepared and used for preconcentration of four sulfonamides (sulfamethoxypyridazine, sulfamethazine, sulfamethoxazole and sulfachloropyridazine) from natural water and milk samples. This material was prepared by sorption of pre-synthesized Fe3O4 nanoparticles (NPs) onto HCP. A number of sorbents with varying Fe3O4NPs content were prepared, and their structural, magnetic and sorption properties were studied. Various experimental parameters affecting the extraction efficiencies such as the amount of the magnetic nanocomposite, extraction time, pH of the sample solution and desorption conditions were studied and optimized. Under the optimal conditions, a convenient and efficient method for the determination of sulfonamides in water and milk samples was developed by combining MSPE and high-performance liquid chromatography with amperometric detection. The results showed that the recoveries of these compounds were in the range of 84-105% with the relative standard deviations ranging between 3% and 10%; the limit of detection were in the range of 0.21-0.33 ng mL(-1) for water and 2.0-2.5 ng mL(-1) for milk.

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Tolmacheva V. V. et al. Facile synthesis of magnetic hypercrosslinked polystyrene and its application in the magnetic solid-phase extraction of sulfonamides from water and milk samples before their HPLC determination // Talanta. 2016. Vol. 152. pp. 203-210.
GOST all authors (up to 50) Copy
Tolmacheva V. V., Apyari V. V., Furletov A. A., Dmitrienko S. G., Zolotov Y. A. Facile synthesis of magnetic hypercrosslinked polystyrene and its application in the magnetic solid-phase extraction of sulfonamides from water and milk samples before their HPLC determination // Talanta. 2016. Vol. 152. pp. 203-210.
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RIS Copy
TY - JOUR
DO - 10.1016/j.talanta.2016.02.010
UR - https://doi.org/10.1016%2Fj.talanta.2016.02.010
TI - Facile synthesis of magnetic hypercrosslinked polystyrene and its application in the magnetic solid-phase extraction of sulfonamides from water and milk samples before their HPLC determination
T2 - Talanta
AU - Apyari, Vladimir V
AU - Zolotov, Yury A
AU - Tolmacheva, Veronika V
AU - Furletov, Aleksei A
AU - Dmitrienko, Stanislava G
PY - 2016
DA - 2016/05/01 00:00:00
PB - Elsevier
SP - 203-210
VL - 152
SN - 0039-9140
SN - 1873-3573
ER -
BibTex
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BibTex Copy
@article{2016_Tolmacheva
author = {Vladimir V Apyari and Yury A Zolotov and Veronika V Tolmacheva and Aleksei A Furletov and Stanislava G Dmitrienko},
title = {Facile synthesis of magnetic hypercrosslinked polystyrene and its application in the magnetic solid-phase extraction of sulfonamides from water and milk samples before their HPLC determination},
journal = {Talanta},
year = {2016},
volume = {152},
publisher = {Elsevier},
month = {may},
url = {https://doi.org/10.1016%2Fj.talanta.2016.02.010},
pages = {203--210},
doi = {10.1016/j.talanta.2016.02.010}
}
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