Synthesis and Complexing Properties of Phosphorus-Substituted Pyridine-2-Carboxylic Acid Anilides
Publication type: Journal Article
Publication date: 2014-08-03
scimago Q4
wos Q3
SJR: 0.264
CiteScore: 2.6
Impact factor: 1.6
ISSN: 10426507, 15635325, 10267719
Organic Chemistry
Biochemistry
Inorganic Chemistry
Abstract
AbstractNovel phosphorus-containing ligands have been synthesized by the condensation of 2-(thio)phosphorylated anilines with 2,6-dichloro- and 4-chloropyridine-2-carbonyl chlorides in the presence of Et3N and unsubstituted pyridine-2-carboxylic acid using P(OPh)3 as a coupling agent. The compounds derived readily form complexes with a range of transition metals (M=Re(I), Pd(II), and Cu(II)), serving as bi- or tridentate monoanionic ligands. The composition and structure of the resulting metallocycles depend both on the presence/amount of the Cl atoms in the pyridine ring and on the nature of the donor atom X in the P=X moiety. The novel compounds were characterized by multinuclear NMR and IR spectroscopy as well as X-ray crystallography.
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V. Aleksanyan D. et al. Synthesis and Complexing Properties of Phosphorus-Substituted Pyridine-2-Carboxylic Acid Anilides // Phosphorus, Sulfur and Silicon and the Related Elements. 2014. Vol. 189. No. 7-8. pp. 1028-1042.
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V. Aleksanyan D., Nelyubina Y. V., Klemenkova Z. S., Kozlov V. A. Synthesis and Complexing Properties of Phosphorus-Substituted Pyridine-2-Carboxylic Acid Anilides // Phosphorus, Sulfur and Silicon and the Related Elements. 2014. Vol. 189. No. 7-8. pp. 1028-1042.
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TY - JOUR
DO - 10.1080/10426507.2014.905571
UR - https://www.tandfonline.com/doi/full/10.1080/10426507.2014.905571
TI - Synthesis and Complexing Properties of Phosphorus-Substituted Pyridine-2-Carboxylic Acid Anilides
T2 - Phosphorus, Sulfur and Silicon and the Related Elements
AU - V. Aleksanyan, Diana
AU - Nelyubina, Yulia V.
AU - Klemenkova, Zinaida S.
AU - Kozlov, Vladimir A
PY - 2014
DA - 2014/08/03
PB - Taylor & Francis
SP - 1028-1042
IS - 7-8
VL - 189
SN - 1042-6507
SN - 1563-5325
SN - 1026-7719
ER -
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@article{2014_V. Aleksanyan,
author = {Diana V. Aleksanyan and Yulia V. Nelyubina and Zinaida S. Klemenkova and Vladimir A Kozlov},
title = {Synthesis and Complexing Properties of Phosphorus-Substituted Pyridine-2-Carboxylic Acid Anilides},
journal = {Phosphorus, Sulfur and Silicon and the Related Elements},
year = {2014},
volume = {189},
publisher = {Taylor & Francis},
month = {aug},
url = {https://www.tandfonline.com/doi/full/10.1080/10426507.2014.905571},
number = {7-8},
pages = {1028--1042},
doi = {10.1080/10426507.2014.905571}
}
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MLA
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V. Aleksanyan, Diana, et al. “Synthesis and Complexing Properties of Phosphorus-Substituted Pyridine-2-Carboxylic Acid Anilides.” Phosphorus, Sulfur and Silicon and the Related Elements, vol. 189, no. 7-8, Aug. 2014, pp. 1028-1042. https://www.tandfonline.com/doi/full/10.1080/10426507.2014.905571.
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