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том 46
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издание 6
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страницы 402-410
Synthesis and Spin State of the Iron(II) Complex with the N,N'-Disubstituted 2,6-Bis(pyrazol-3-yl)pyridine Ligand
Тип публикации: Journal Article
Дата публикации: 2020-06-14
scimago Q4
wos Q4
БС2
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Краткое описание
The reaction of a new tridentate ligand 2,6-bis(5-tert-butyl-1-(2,6-difluorophenyl)-1H-pyrazol-3-yl)pyridine (L) with the divalent iron salt affords the iron(II) complex [Fe(L)2](BF4)2 (I), which is isolated in the individual state and characterized by elemental analysis, NMR spectroscopy, and X-ray diffraction analysis. According to the X-ray diffraction results and data of the Evans method, which makes it possible to determine the spin state of paramagnetic compounds in a solution from the NMR spectra, the iron(II) ion in complex I exists in the high-spin state (S = 2 for Fe(II)) and undergoes no temperature-induced spin transition in a range of 120–345 K.
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Nikovskii I. A. et al. Synthesis and Spin State of the Iron(II) Complex with the N,N'-Disubstituted 2,6-Bis(pyrazol-3-yl)pyridine Ligand // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2020. Vol. 46. No. 6. pp. 402-410.
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Nikovskii I. A., Polezhaev A. V., Aleshin D. Yu., Melnikova E. K., Nelyubina Yu. V. Synthesis and Spin State of the Iron(II) Complex with the N,N'-Disubstituted 2,6-Bis(pyrazol-3-yl)pyridine Ligand // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2020. Vol. 46. No. 6. pp. 402-410.
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TY - JOUR
DO - 10.1134/S107032842006007X
UR - https://doi.org/10.1134/S107032842006007X
TI - Synthesis and Spin State of the Iron(II) Complex with the N,N'-Disubstituted 2,6-Bis(pyrazol-3-yl)pyridine Ligand
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Nikovskii, I A
AU - Polezhaev, A V
AU - Aleshin, D Yu
AU - Melnikova, E K
AU - Nelyubina, Yu V
PY - 2020
DA - 2020/06/14
PB - Pleiades Publishing
SP - 402-410
IS - 6
VL - 46
SN - 1070-3284
SN - 1608-3318
ER -
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@article{2020_Nikovskii,
author = {I A Nikovskii and A V Polezhaev and D Yu Aleshin and E K Melnikova and Yu V Nelyubina},
title = {Synthesis and Spin State of the Iron(II) Complex with the N,N'-Disubstituted 2,6-Bis(pyrazol-3-yl)pyridine Ligand},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2020},
volume = {46},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://doi.org/10.1134/S107032842006007X},
number = {6},
pages = {402--410},
doi = {10.1134/S107032842006007X}
}
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Nikovskii, I. A., et al. “Synthesis and Spin State of the Iron(II) Complex with the N,N'-Disubstituted 2,6-Bis(pyrazol-3-yl)pyridine Ligand.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 46, no. 6, Jun. 2020, pp. 402-410. https://doi.org/10.1134/S107032842006007X.
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