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Synthesis of 1,3-bis(trimethylcyclam) and 1,3-bis(trimethylcyclen) substituted benzenes
Тип публикации: Journal Article
Дата публикации: 2009-01-01
Включен в RSCI
scimago Q4
wos Q3
БС2
SJR: 0.193
CiteScore: 1.5
Impact factor: 1.2
ISSN: 19989539, 27131092
Organic Chemistry
Analytical Chemistry
Краткое описание
Pd-catalyzed amination of 1,3-dibromobenzene with N,N',N''-trimethylcyclam and N,N',N''-trimethylcyclen provided corresponding 1,3-bis(tetraazamacrocyclic) derivatives of benzene in 25-32% yields. The dependence of the products yields on the phosphine ligand applied (BINAP, DavePHOS) as well as on the stoichiometry of starting compounds was established. Scope and limitations for the synthesis of N-phenyl and N-(3-bromophenyl) derivatives of trimethylcyclam and trimethylcyclen were demonstrated.
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Averin A. D. et al. Synthesis of 1,3-bis(trimethylcyclam) and 1,3-bis(trimethylcyclen) substituted benzenes // Macroheterocycles. 2009. Vol. 2. No. 3-4. pp. 281-285.
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Averin A. D., Shukhaev A. V., Buryak A. K., Denat F., Guilard R., Beletskaya I. P. Synthesis of 1,3-bis(trimethylcyclam) and 1,3-bis(trimethylcyclen) substituted benzenes // Macroheterocycles. 2009. Vol. 2. No. 3-4. pp. 281-285.
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TY - JOUR
DO - 10.6060/mhc2009.3-4.281
UR - https://doi.org/10.6060/mhc2009.3-4.281
TI - Synthesis of 1,3-bis(trimethylcyclam) and 1,3-bis(trimethylcyclen) substituted benzenes
T2 - Macroheterocycles
AU - Averin, Alexei D.
AU - Shukhaev, Anton V
AU - Buryak, Alexei K.
AU - Denat, Franck
AU - Guilard, Roger
AU - Beletskaya, Irina P.
PY - 2009
DA - 2009/01/01
PB - Ivanovo State University of Chemistry and Technology
SP - 281-285
IS - 3-4
VL - 2
SN - 1998-9539
SN - 2713-1092
ER -
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@article{2009_Averin,
author = {Alexei D. Averin and Anton V Shukhaev and Alexei K. Buryak and Franck Denat and Roger Guilard and Irina P. Beletskaya},
title = {Synthesis of 1,3-bis(trimethylcyclam) and 1,3-bis(trimethylcyclen) substituted benzenes},
journal = {Macroheterocycles},
year = {2009},
volume = {2},
publisher = {Ivanovo State University of Chemistry and Technology},
month = {jan},
url = {https://doi.org/10.6060/mhc2009.3-4.281},
number = {3-4},
pages = {281--285},
doi = {10.6060/mhc2009.3-4.281}
}
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MLA
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Averin, Alexei D., et al. “Synthesis of 1,3-bis(trimethylcyclam) and 1,3-bis(trimethylcyclen) substituted benzenes.” Macroheterocycles, vol. 2, no. 3-4, Jan. 2009, pp. 281-285. https://doi.org/10.6060/mhc2009.3-4.281.
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