Inorganic Materials, volume 56, issue 7, pages 700-706
Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials
Fadeeva I. V.
1
,
Fomin A.S.
1
,
Barinov S. M.
1
,
Davydova G A
2
,
Selezneva I I
2
,
Preobrazhenskii I I
3
,
Rusakov M K
4
,
Fomina A A
1
,
Volchenkova V A
1
Publication type: Journal Article
Publication date: 2020-07-28
Journal:
Inorganic Materials
Quartile SCImago
Q3
Quartile WOS
Q4
Impact factor: 0.8
ISSN: 00201685, 16083172
Materials Chemistry
Metals and Alloys
Inorganic Chemistry
General Chemical Engineering
Abstract
We have studied manganese-containing calcium phosphates differing in manganese content and phase composition. At a manganese content of 0.15 wt %, the whitlockite content is ~90 wt % and the calcium pyrophosphate content is ~10 wt %. Increasing the manganese content to 1.49 wt % reduces the whitlockite content to ~70 wt % and increases the calcium pyrophosphate content to ~30 wt %. IR spectroscopy results show that the samples calcined at 400°C have the apatite structure, whereas raising the calcination temperature to 900°C leads to the formation of the whitlockite structure and calcium pyrophosphate. Active sintering begins in the range 920–1050°C. Raising the firing temperature to 1200°C leads to the formation of a densely sintered structure, with melted regions and an average grain size from 15 to 25 μm. With increasing manganese content, the grain size of the ceramics decreases. Our results on cytotoxic properties demonstrate that the samples are not cytotoxic and maintain cell proliferation and spreading. The cytotoxicity of the samples is insensitive to the calcium pyrophosphate and manganese concentrations. The powders and ceramics prepared in this study can be used as key components of novel materials for bone tissue engineering.
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Fadeeva I. V. et al. Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials // Inorganic Materials. 2020. Vol. 56. No. 7. pp. 700-706.
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Fadeeva I. V., Fomin A., Barinov S. M., Davydova G. A., Selezneva I. I., Preobrazhenskii I. I., Rusakov M. K., Fomina A. A., Volchenkova V. A. Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials // Inorganic Materials. 2020. Vol. 56. No. 7. pp. 700-706.
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TY - JOUR
DO - 10.1134/S0020168520070055
UR - https://doi.org/10.1134%2FS0020168520070055
TI - Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials
T2 - Inorganic Materials
AU - Fadeeva, I. V.
AU - Fomin, A.S.
AU - Barinov, S. M.
AU - Davydova, G A
AU - Selezneva, I I
AU - Preobrazhenskii, I I
AU - Rusakov, M K
AU - Fomina, A A
AU - Volchenkova, V A
PY - 2020
DA - 2020/07/28 00:00:00
PB - Pleiades Publishing
SP - 700-706
IS - 7
VL - 56
SN - 0020-1685
SN - 1608-3172
ER -
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@article{2020_Fadeeva,
author = {I. V. Fadeeva and A.S. Fomin and S. M. Barinov and G A Davydova and I I Selezneva and I I Preobrazhenskii and M K Rusakov and A A Fomina and V A Volchenkova},
title = {Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials},
journal = {Inorganic Materials},
year = {2020},
volume = {56},
publisher = {Pleiades Publishing},
month = {jul},
url = {https://doi.org/10.1134%2FS0020168520070055},
number = {7},
pages = {700--706},
doi = {10.1134/S0020168520070055}
}
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Fadeeva, I. V., et al. “Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials.” Inorganic Materials, vol. 56, no. 7, Jul. 2020, pp. 700-706. https://doi.org/10.1134%2FS0020168520070055.