Open Access
MolBank, volume 2021, issue 3, pages M1247
Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate
Chmovzh Timofey N
1, 2
,
Rakitin Oleg A.
1, 2
Publication type: Journal Article
Publication date: 2021-07-05
DOI:
10.3390/M1247
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
New donor building blocks, i.e., triarylamino derivatives, are of great interest for the production of organic photovoltaic materials. In this communication, bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)amine was synthesized in a two-step process via hydrolysis of its tert-butyl carbamate derivative. tert-Butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate was obtained by Suzuki cross-coupling reaction of tert-butyl bis(4-bromophenyl)carbamate and (4-(hexyloxy)phenyl)boronic acid in the presence of tetrakis(triphenylphosphine)palladium(0). The structure of newly synthesized compounds was established by means of elemental analysis, high resolution mass-spectrometry, 1H, 13C-NMR, IR and UV spectroscopy and mass-spectrometry.
Citations by journals
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MolBank
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MolBank
1 publication, 100%
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1
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Citations by publishers
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Multidisciplinary Digital Publishing Institute (MDPI)
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Multidisciplinary Digital Publishing Institute (MDPI)
1 publication, 100%
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1
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Chmovzh T. N. et al. Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate // MolBank. 2021. Vol. 2021. No. 3. p. M1247.
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Chmovzh T. N., Rakitin O. A. Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate // MolBank. 2021. Vol. 2021. No. 3. p. M1247.
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TY - JOUR
DO - 10.3390/M1247
UR - https://doi.org/10.3390%2FM1247
TI - Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate
T2 - MolBank
AU - Chmovzh, Timofey N
AU - Rakitin, Oleg A.
PY - 2021
DA - 2021/07/05 00:00:00
PB - Multidisciplinary Digital Publishing Institute (MDPI)
SP - M1247
IS - 3
VL - 2021
SN - 1422-8599
ER -
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@article{2021_Chmovzh
author = {Timofey N Chmovzh and Oleg A. Rakitin},
title = {Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate},
journal = {MolBank},
year = {2021},
volume = {2021},
publisher = {Multidisciplinary Digital Publishing Institute (MDPI)},
month = {jul},
url = {https://doi.org/10.3390%2FM1247},
number = {3},
pages = {M1247},
doi = {10.3390/M1247}
}
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Chmovzh, Timofey N., et al. “Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate.” MolBank, vol. 2021, no. 3, Jul. 2021, p. M1247. https://doi.org/10.3390%2FM1247.
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