Russian Journal of General Chemistry, volume 90, issue 12, pages 2323-2327

Composition and Structure of Complexes Formed in GeCl4–2-Hydroxybenzene(2-hydroxynaphthaline-1)carbaldehyde Isonicotinoylhydrazone–ZnCl2–Methanol

Shmatkova N V 1
, 
Seifullina I I 1
, 
Skorokhod L S 1
, 
Morozov A. N. 2
, 
POPOV L.D. 2
, 
Gazieva G A 3
1
 
Mechnikov Odessa National University, Odessa, Ukraine | 
2
 
3
 
Publication type: Journal Article
Publication date: 2020-12-01
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ISSN: 10703632, 16083350
General Chemistry
Abstract
Tetrachlorozincates [Ge(LH)2][ZnCl4]∙CH3OH were isolated for the first time from isonicotinoylhydrazone 2-hydroxybenzene (2-hydroxynaphyl-1)carbaldehyde (H2L)–GeCl4–ZnCl2–CH3OH systems, in which cations are [Ge(L·H)2]2+ complexes protonated by the pyridine nitrogen atom, with L ligands tridentately coordinated via the azomethine nitrogen atom and oxygen atoms of deprotonated hydroxyazino and hydroxy groups. The complexes were studied using the methods of conductometry, thermogravimetry, IR, and 1H NMR spectroscopy.
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Shmatkova N. V. et al. Composition and Structure of Complexes Formed in GeCl4–2-Hydroxybenzene(2-hydroxynaphthaline-1)carbaldehyde Isonicotinoylhydrazone–ZnCl2–Methanol // Russian Journal of General Chemistry. 2020. Vol. 90. No. 12. pp. 2323-2327.
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Shmatkova N. V., Seifullina I. I., Skorokhod L. S., Morozov A. N., POPOV L., Gazieva G. A. Composition and Structure of Complexes Formed in GeCl4–2-Hydroxybenzene(2-hydroxynaphthaline-1)carbaldehyde Isonicotinoylhydrazone–ZnCl2–Methanol // Russian Journal of General Chemistry. 2020. Vol. 90. No. 12. pp. 2323-2327.
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TY - JOUR
DO - 10.1134/S1070363220120154
UR - https://doi.org/10.1134%2FS1070363220120154
TI - Composition and Structure of Complexes Formed in GeCl4–2-Hydroxybenzene(2-hydroxynaphthaline-1)carbaldehyde Isonicotinoylhydrazone–ZnCl2–Methanol
T2 - Russian Journal of General Chemistry
AU - Shmatkova, N V
AU - Seifullina, I I
AU - Skorokhod, L S
AU - Morozov, A. N.
AU - Gazieva, G A
AU - POPOV, L.D.
PY - 2020
DA - 2020/12/01 00:00:00
PB - Pleiades Publishing
SP - 2323-2327
IS - 12
VL - 90
SN - 1070-3632
SN - 1608-3350
ER -
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@article{2020_Shmatkova,
author = {N V Shmatkova and I I Seifullina and L S Skorokhod and A. N. Morozov and G A Gazieva and L.D. POPOV},
title = {Composition and Structure of Complexes Formed in GeCl4–2-Hydroxybenzene(2-hydroxynaphthaline-1)carbaldehyde Isonicotinoylhydrazone–ZnCl2–Methanol},
journal = {Russian Journal of General Chemistry},
year = {2020},
volume = {90},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134%2FS1070363220120154},
number = {12},
pages = {2323--2327},
doi = {10.1134/S1070363220120154}
}
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Shmatkova, N. V., et al. “Composition and Structure of Complexes Formed in GeCl4–2-Hydroxybenzene(2-hydroxynaphthaline-1)carbaldehyde Isonicotinoylhydrazone–ZnCl2–Methanol.” Russian Journal of General Chemistry, vol. 90, no. 12, Dec. 2020, pp. 2323-2327. https://doi.org/10.1134%2FS1070363220120154.
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