Tetrahedron Letters, volume 60, issue 17, pages 1174-1178

Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology

Publication typeJournal Article
Publication date2019-04-01
Quartile SCImago
Q3
Quartile WOS
Q3
Impact factor1.8
ISSN00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
Abstract New gelling agents have been discovered: glycoluril carboxylic acid amides, giving two-component gels with imidazole. First, the one-pot, two step reaction of glycoluril carboxylic acids, CDI and various amines was investigated for the preparation of gels and it was found that the reaction mixtures were gelled in dry DMF during the preparation of some amides. The conditions of the gel-sol-gel transitions were found. The morphology of the xerogels was studied by SEM. The structure of the xerogels is constructed from interlocked rods or from interlaced curved fibres. Self-organization in the co-crystals of amides with H2O or imidazole was detected. The molecules of the co-crystals of amides with H2O are self-assembled into homochiral tapes.

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Baranov P. G. et al. Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology // Tetrahedron Letters. 2019. Vol. 60. No. 17. pp. 1174-1178.
GOST all authors (up to 50) Copy
Baranov P. G., Baganova A. A., Chikunov I. E., Karnoukhova V. A., Kravchenko A. N. Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology // Tetrahedron Letters. 2019. Vol. 60. No. 17. pp. 1174-1178.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.tetlet.2019.03.053
UR - https://doi.org/10.1016%2Fj.tetlet.2019.03.053
TI - Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology
T2 - Tetrahedron Letters
AU - Baranov, Pavel G.
AU - Baganova, Anastasiya A
AU - Chikunov, Il’ya E.
AU - Karnoukhova, Valentina A
AU - Kravchenko, Angelina N.
PY - 2019
DA - 2019/04/01 00:00:00
PB - Elsevier
SP - 1174-1178
IS - 17
VL - 60
SN - 0040-4039
SN - 1873-3581
ER -
BibTex |
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BibTex Copy
@article{2019_Baranov
author = {Pavel G. Baranov and Anastasiya A Baganova and Il’ya E. Chikunov and Valentina A Karnoukhova and Angelina N. Kravchenko},
title = {Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology},
journal = {Tetrahedron Letters},
year = {2019},
volume = {60},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016%2Fj.tetlet.2019.03.053},
number = {17},
pages = {1174--1178},
doi = {10.1016/j.tetlet.2019.03.053}
}
MLA
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MLA Copy
Baranov, Pavel G., et al. “Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology.” Tetrahedron Letters, vol. 60, no. 17, Apr. 2019, pp. 1174-1178. https://doi.org/10.1016%2Fj.tetlet.2019.03.053.
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