Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, volume 265, issue 1, pages 334-338
The peculiarities of formation of the metal nanoparticles in irradiated polymer metal complexes
Zezin A.
1
,
Feldman Vladimir I.
1, 2
,
Shmakova Nina L.
1
,
Valueva S P
3
,
Ivanchenko V K
1
,
Nikanorova N I
3
Publication type: Journal Article
Publication date: 2007-12-01
Quartile SCImago
Q2
Quartile WOS
Q3
Impact factor: 1.3
ISSN: 0168583X
Instrumentation
Nuclear and High Energy Physics
Abstract
Abstract The radiation-induced reduction of metal ions in the films of triple metal polymer complexes of polyacrylic acid–polyethyleneimine–copper(II) or nickel(II) (PAA–PEI–Cu2+ or PAA–PEI–Ni2+) was studied by EPR and transmission electron microscopy (TEM). It was shown that irradiation of the swollen polymer films in the water–alcohol environment resulted in effective reduction of the metal ions. The exchange between the swollen film and outer environment was found to be an important factor for ion reduction and stabilization of metal particles. EPR data have revealed pronounced effect of the ligand environment on the reduction efficiency. The electron microscopy studies have demonstrated that the dimensions of main fraction of metal particles obtained by the radiation-chemical reduction are in the range of 2–2.5 nm both for Cu and for Ni complexes.
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Citations by publishers
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Zezin A. et al. The peculiarities of formation of the metal nanoparticles in irradiated polymer metal complexes // Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms. 2007. Vol. 265. No. 1. pp. 334-338.
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Zezin A., Feldman V. I., Shmakova N. L., Valueva S. P., Ivanchenko V. K., Nikanorova N. I. The peculiarities of formation of the metal nanoparticles in irradiated polymer metal complexes // Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms. 2007. Vol. 265. No. 1. pp. 334-338.
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TY - JOUR
DO - 10.1016/j.nimb.2007.08.068
UR - https://doi.org/10.1016%2Fj.nimb.2007.08.068
TI - The peculiarities of formation of the metal nanoparticles in irradiated polymer metal complexes
T2 - Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms
AU - Zezin, A.
AU - Feldman, Vladimir I.
AU - Shmakova, Nina L.
AU - Valueva, S P
AU - Ivanchenko, V K
AU - Nikanorova, N I
PY - 2007
DA - 2007/12/01 00:00:00
PB - Elsevier
SP - 334-338
IS - 1
VL - 265
SN - 0168-583X
ER -
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@article{2007_Zezin,
author = {A. Zezin and Vladimir I. Feldman and Nina L. Shmakova and S P Valueva and V K Ivanchenko and N I Nikanorova},
title = {The peculiarities of formation of the metal nanoparticles in irradiated polymer metal complexes},
journal = {Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms},
year = {2007},
volume = {265},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016%2Fj.nimb.2007.08.068},
number = {1},
pages = {334--338},
doi = {10.1016/j.nimb.2007.08.068}
}
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Zezin, A., et al. “The peculiarities of formation of the metal nanoparticles in irradiated polymer metal complexes.” Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, vol. 265, no. 1, Dec. 2007, pp. 334-338. https://doi.org/10.1016%2Fj.nimb.2007.08.068.