Open Access
MolBank, volume 2020, issue 3, pages M1149
Ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][ 1,4]oxazine-5a(6h)-carboxylate
Publication type: Journal Article
Publication date: 2020-07-21
DOI:
10.3390/M1149
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
The 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][1,4]oxazine heterocyclic system has been used in the construction of heteropropellanes, which attracted much attention not only on the possible modification of drugs, but also for novel materials with unusual and important physical properties. In this communication, the reaction of ethyl 2-(hydroxyimino)propanoate 1 with disulfur dichloride and o-aminophenol, which gave ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][1,4]oxazine-5a(6H)-carboxylate in moderate yield, was described. The structure of the newly synthesized compound was established by means of elemental analysis, high resolution mass-spectrometry, 1H, 13C NMR and IR spectroscopy, mass-spectrometry and X-ray analysis.
Citations by journals
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1
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Acta Crystallographica Section E: Crystallographic Communications
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Acta Crystallographica Section E: Crystallographic Communications
1 publication, 50%
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MolBank
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MolBank
1 publication, 50%
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1
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Citations by publishers
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1
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International Union of Crystallography (IUCr)
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International Union of Crystallography (IUCr)
1 publication, 50%
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Multidisciplinary Digital Publishing Institute (MDPI)
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Multidisciplinary Digital Publishing Institute (MDPI)
1 publication, 50%
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1
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Konstantinova L. S. et al. Ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][ 1,4]oxazine-5a(6h)-carboxylate // MolBank. 2020. Vol. 2020. No. 3. p. M1149.
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Konstantinova L. S., Tolmachev M. A., Popov V. V., Rakitin O. A. Ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][ 1,4]oxazine-5a(6h)-carboxylate // MolBank. 2020. Vol. 2020. No. 3. p. M1149.
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TY - JOUR
DO - 10.3390/M1149
UR - https://doi.org/10.3390%2FM1149
TI - Ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][ 1,4]oxazine-5a(6h)-carboxylate
T2 - MolBank
AU - Konstantinova, Lidia S.
AU - Popov, Vadim V
AU - Tolmachev, Mikhail A
AU - Rakitin, Oleg A.
PY - 2020
DA - 2020/07/21 00:00:00
PB - Multidisciplinary Digital Publishing Institute (MDPI)
SP - M1149
IS - 3
VL - 2020
SN - 1422-8599
ER -
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@article{2020_Konstantinova,
author = {Lidia S. Konstantinova and Vadim V Popov and Mikhail A Tolmachev and Oleg A. Rakitin},
title = {Ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][ 1,4]oxazine-5a(6h)-carboxylate},
journal = {MolBank},
year = {2020},
volume = {2020},
publisher = {Multidisciplinary Digital Publishing Institute (MDPI)},
month = {jul},
url = {https://doi.org/10.3390%2FM1149},
number = {3},
pages = {M1149},
doi = {10.3390/M1149}
}
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Konstantinova, Lidia S., et al. “Ethyl 11a,12-dihydrobenzo[b]benzo[5,6][1,4]oxazino[2,3-e][ 1,4]oxazine-5a(6h)-carboxylate.” MolBank, vol. 2020, no. 3, Jul. 2020, p. M1149. https://doi.org/10.3390%2FM1149.