Open Access
MolBank, volume 2019, issue 1, pages M1053
3,6-dibromopyridazine-4,5-diamine
Publication type: Journal Article
Publication date: 2019-03-21
DOI:
10.3390/M1053
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
Dihalogenated derivatives of 1,2,5-chalcogenadiazoles fused with benzene or heterocyclic rings are of interest as starting compounds for photovoltaic materials. The 1,2,5-chalcogenadiazole ring in these heterocycles was most commonly prepared from the corresponding ortho-diamine moiety. In this communication, 3,6-dibromopyridazine-4,5-diamine was prepared via the reaction of 4,7-dibromo[1,2,5]thiadiazolo[3,4-d]pyridazine with sodium methoxide in THF by heating at reflux for four hours. The structure of the newly synthesized compound was established by means of high resolution mass-spectrometry, 1H, 13C-NMR and IR spectroscopy, and mass-spectrometry.
Citations by journals
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MolBank
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MolBank
1 publication, 50%
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Multidisciplinary Digital Publishing Institute (MDPI)
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Multidisciplinary Digital Publishing Institute (MDPI)
1 publication, 50%
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1
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TY - JOUR
DO - 10.3390/M1053
UR - https://doi.org/10.3390%2FM1053
TI - 3,6-dibromopyridazine-4,5-diamine
T2 - MolBank
AU - Chmovzh, Timofey
AU - Knyazeva, Ekaterina
AU - Ustimenko, Olga
AU - Rakitin, Oleg
PY - 2019
DA - 2019/03/21 00:00:00
PB - Multidisciplinary Digital Publishing Institute (MDPI)
SP - M1053
IS - 1
VL - 2019
SN - 1422-8599
ER -
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@article{2019_Chmovzh,
author = {Timofey Chmovzh and Ekaterina Knyazeva and Olga Ustimenko and Oleg Rakitin},
title = {3,6-dibromopyridazine-4,5-diamine},
journal = {MolBank},
year = {2019},
volume = {2019},
publisher = {Multidisciplinary Digital Publishing Institute (MDPI)},
month = {mar},
url = {https://doi.org/10.3390%2FM1053},
number = {1},
pages = {M1053},
doi = {10.3390/M1053}
}
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Chmovzh, Timofey, et al. “3,6-dibromopyridazine-4,5-diamine.” MolBank, vol. 2019, no. 1, Mar. 2019, p. M1053. https://doi.org/10.3390%2FM1053.