Open Access
MolBank, volume 2018, issue 1, pages M982
4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide
Publication type: Journal Article
Publication date: 2018-02-18
DOI:
10.3390/M982
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
Dihalogenated derivatives of [1,2,5]chalcogenadiazolo[3,4-d]pyridazines are of interest as precursors for both photovoltaic materials and biologically active compounds. In this communication, 4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide was prepared via the reaction of 3,6-dichloro-5-nitropyridazin-4-amine with oxidizing agents; the best yield of the target compound was achieved in the reaction with (diacetoxyiodo)benzene in benzene by heating at reflux for two hours. The structure of the newly synthesized compound was established by means of 13C-NMR and IR spectroscopy, mass-spectrometry and elemental analysis.
Citations by journals
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1
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MolBank
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MolBank
1 publication, 25%
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Journal of the American Chemical Society
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Journal of the American Chemical Society
1 publication, 25%
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Crystal Growth and Design
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Crystal Growth and Design
1 publication, 25%
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1
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Citations by publishers
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1
2
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American Chemical Society (ACS)
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American Chemical Society (ACS)
2 publications, 50%
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Multidisciplinary Digital Publishing Institute (MDPI)
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Multidisciplinary Digital Publishing Institute (MDPI)
1 publication, 25%
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1
2
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Chmovzh T. et al. 4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide // MolBank. 2018. Vol. 2018. No. 1. p. M982.
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Chmovzh T., Knyazeva E., Popov V., Rakitin O. A. 4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide // MolBank. 2018. Vol. 2018. No. 1. p. M982.
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TY - JOUR
DO - 10.3390/M982
UR - https://doi.org/10.3390%2FM982
TI - 4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide
T2 - MolBank
AU - Chmovzh, Timofey
AU - Knyazeva, Ekaterina
AU - Popov, Vadim
AU - Rakitin, Oleg A.
PY - 2018
DA - 2018/02/18 00:00:00
PB - Multidisciplinary Digital Publishing Institute (MDPI)
SP - M982
IS - 1
VL - 2018
SN - 1422-8599
ER -
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@article{2018_Chmovzh,
author = {Timofey Chmovzh and Ekaterina Knyazeva and Vadim Popov and Oleg A. Rakitin},
title = {4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide},
journal = {MolBank},
year = {2018},
volume = {2018},
publisher = {Multidisciplinary Digital Publishing Institute (MDPI)},
month = {feb},
url = {https://doi.org/10.3390%2FM982},
number = {1},
pages = {M982},
doi = {10.3390/M982}
}
Cite this
MLA
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Chmovzh, Timofey, et al. “4,7-dichloro[1,2,5]oxadiazolo[3,4-d]pyridazine 1-oxide.” MolBank, vol. 2018, no. 1, Feb. 2018, p. M982. https://doi.org/10.3390%2FM982.