Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry
Тип публикации: Journal Article
Дата публикации: 2002-06-01
SCImago Q2
WOS Q2
БС2
SJR: 0.553
CiteScore: 6.5
Impact factor: 3.6
ISSN: 16159306, 16159314
Analytical Chemistry
Filtration and Separation
Краткое описание
A method for determination of residual styrene monomer and other volatile organic compounds in expanded polystyrene (EPS) was developed using HS SPME and gas chromatography with FID. The extraction products were identified by GC/MS. Good reproducibility of the measurements with RSD values between 3.2–3.6% was achieved by extraction using a 75 μm Carboxen-Polydimethylsiloxane fiber at 60°C with 15 min sample sonication. The contents of residual styrene monomer in two samples of EPS were 153.2 and 65.7 mg/kg, respectively. Other compounds identified in EPS were pentane, benzene, toluene, ethylbenzene, isomers of xylene, n-propylbenzene, 1,2,4-trimethylbenzene, o-methylstyrene, benzaldehyde, benzyl alcohol, and acetophenone.
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Kusch P., Knupp G. Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry // Journal of Separation Science. 2002. Vol. 25. No. 8. pp. 539-542.
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Kusch P., Knupp G. Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry // Journal of Separation Science. 2002. Vol. 25. No. 8. pp. 539-542.
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TY - JOUR
DO - 10.1002/1615-9314(20020601)25:8<539::aid-jssc539>3.0.co;2-g
UR - https://doi.org/10.1002/1615-9314(20020601)25:8<539::aid-jssc539>3.0.co;2-g
TI - Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry
T2 - Journal of Separation Science
AU - Kusch, Peter
AU - Knupp, Gerd
PY - 2002
DA - 2002/06/01
PB - Wiley
SP - 539-542
IS - 8
VL - 25
SN - 1615-9306
SN - 1615-9314
ER -
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@article{2002_Kusch,
author = {Peter Kusch and Gerd Knupp},
title = {Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry},
journal = {Journal of Separation Science},
year = {2002},
volume = {25},
publisher = {Wiley},
month = {jun},
url = {https://doi.org/10.1002/1615-9314(20020601)25:8<539::aid-jssc539>3.0.co;2-g},
number = {8},
pages = {539--542},
doi = {10.1002/1615-9314(20020601)25:8<539::aid-jssc539>3.0.co;2-g}
}
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MLA
Скопировать
Kusch, Peter, and Gerd Knupp. “Analysis of residual styrene monomer and other volatile organic compounds in expanded polystyrene by headspace solid-phase microextraction followed by gas chromatography and gas chromatography/mass spectrometry.” Journal of Separation Science, vol. 25, no. 8, Jun. 2002, pp. 539-542. https://doi.org/10.1002/1615-9314(20020601)25:8<539::aid-jssc539>3.0.co;2-g.
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