Advanced Synthesis and Catalysis, volume 356, issue 14-15, pages 3092-3098

Heterogeneous Copper-Catalyzed Cascade Three-Component Reaction of Amines, Carbon Disulfide and 2-Iodoanilines Leading to 2-Aminobenzothiazoles

Hong Zhao ^{1, 2}

He Wen ³

Ruiya Yao ³

Mingzhong Cai ³

Key Laboratory of Functional Small Organic Molecule, Ministry of Education and College of Chemistry & Chemical Engineering, Jiangxi Normal University, Nanchang 330022, People's Republic of China, Fax: (+86)-791-8812-0388 |

School of Chemistry and Chemical Engineering, GuangDong Pharmaceutical University, Guangzhou 510006, People's Republic of China |

Publication type: Journal Article

Publication date: 2014-09-21

Wiley

Journal: Advanced Synthesis and Catalysis

scimago Q1

SJR: 1.020

CiteScore: 9.4

Impact factor: 4.4

ISSN: 16154150, 16154169

DOI: 10.1002/adsc.201400381

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General Chemistry

Abstract

The heterogeneous cascade three-component reaction of amines, carbon disulfide (CS2) and 2-iodoanilines was achieved in dimethylformamide (DMF) at 110 °C in the presence of 10 mol% of 3-(2-aminoethylamino)propyl-functionalized MCM-41-immobilized copper complex [MCM-41-2N-CuCl] using potassium carbonate (K2CO3) as base, yielding a variety of 2-aminobenzothiazoles in good to excellent yields. This heterogeneous copper catalyst influences the selectivity of the reaction and can be recovered and recycled by a simple filtration of the reaction solution and used for at least 10 consecutive trials without any decreases in activity.

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Publisher

Wiley

Journal

Advanced Synthesis and Catalysis

scimago Q1

SJR

1.020

CiteScore

9.4

Impact factor

4.4

ISSN

16154150 (Print)

16154169 (Electronic)

Heterogeneous Copper-Catalyzed Cascade Three-Component Reaction of Amines, Carbon Disulfide and 2-Iodoanilines Leading to 2-Aminobenzothiazoles

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