volume 7 issue 12 pages 2872-2881

Synthesis and Structure-Activity Relationship of Vicenistatin, a Cytotoxic 20-Membered Macrolactam Glycoside

Publication typeJournal Article
Publication date2012-09-27
scimago Q2
wos Q2
SJR0.751
CiteScore5.9
Impact factor3.3
ISSN18614728, 1861471X
General Chemistry
Organic Chemistry
Biochemistry
Abstract
We have developed two syntheses of vicenistatin and its analogues. Our first-generation strategy included the rapid and sequential assembly of the macrocyclic lactam by using an intermolecular Horner-Wadsworth-Emmons reaction between the C3-C13 fragment and the C1-C2, C14-C19 fragment, followed by an intramolecular Stille coupling reaction. The second-generation strategy utilized a ring-closing metathesis of a hexaene intermediate to generate the desired 20-membered macrolactam. This second-generation strategy made it possible to prepare synthetic analogues of vicenistatin, including the C20- and/or C23-demethyl analogues. Evaluation of the cytotoxic effect of these analogues indicated the importance of the fixed conformation of aglycon for determining the biological activity of the vicenistatins.
Found 
Found 

Top-30

Journals

1
Yuki Gosei Kagaku Kyokaishi/Journal of Synthetic Organic Chemistry
1 publication, 6.67%
Bioorganic and Medicinal Chemistry Letters
1 publication, 6.67%
Tetrahedron
1 publication, 6.67%
Coordination Chemistry Reviews
1 publication, 6.67%
European Journal of Medicinal Chemistry
1 publication, 6.67%
Chemistry - A European Journal
1 publication, 6.67%
European Journal of Organic Chemistry
1 publication, 6.67%
Organic Letters
1 publication, 6.67%
Journal of Organic Chemistry
1 publication, 6.67%
Chemical Communications
1 publication, 6.67%
Natural Product Reports
1 publication, 6.67%
Topics in Heterocyclic Chemistry
1 publication, 6.67%
Synlett
1 publication, 6.67%
Journal of Antibiotics
1 publication, 6.67%
Science advances
1 publication, 6.67%
1

Publishers

1
2
3
4
Elsevier
4 publications, 26.67%
Wiley
2 publications, 13.33%
American Chemical Society (ACS)
2 publications, 13.33%
Royal Society of Chemistry (RSC)
2 publications, 13.33%
Springer Nature
2 publications, 13.33%
The Society of Synthetic Organic Chemistry, Japan
1 publication, 6.67%
Georg Thieme Verlag KG
1 publication, 6.67%
American Association for the Advancement of Science (AAAS)
1 publication, 6.67%
1
2
3
4
  • We do not take into account publications without a DOI.
  • Statistics recalculated weekly.

Are you a researcher?

Create a profile to get free access to personal recommendations for colleagues and new articles.
Metrics
15
Share
Cite this
GOST |
Cite this
GOST Copy
Fukuda H. et al. Synthesis and Structure-Activity Relationship of Vicenistatin, a Cytotoxic 20-Membered Macrolactam Glycoside // Chemistry - An Asian Journal. 2012. Vol. 7. No. 12. pp. 2872-2881.
GOST all authors (up to 50) Copy
Fukuda H., Nishiyama Y., Nakamura S., Ohno Y., Eguchi T., Iwabuchi Y., USUI T., Kanoh N. Synthesis and Structure-Activity Relationship of Vicenistatin, a Cytotoxic 20-Membered Macrolactam Glycoside // Chemistry - An Asian Journal. 2012. Vol. 7. No. 12. pp. 2872-2881.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1002/asia.201200615
UR - https://doi.org/10.1002/asia.201200615
TI - Synthesis and Structure-Activity Relationship of Vicenistatin, a Cytotoxic 20-Membered Macrolactam Glycoside
T2 - Chemistry - An Asian Journal
AU - Fukuda, Hayato
AU - Nishiyama, Yuko
AU - Nakamura, Shiina
AU - Ohno, Yutaro
AU - Eguchi, T.
AU - Iwabuchi, Yoshiharu
AU - USUI, TAKEO
AU - Kanoh, Naoki
PY - 2012
DA - 2012/09/27
PB - Wiley
SP - 2872-2881
IS - 12
VL - 7
PMID - 23015368
SN - 1861-4728
SN - 1861-471X
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2012_Fukuda,
author = {Hayato Fukuda and Yuko Nishiyama and Shiina Nakamura and Yutaro Ohno and T. Eguchi and Yoshiharu Iwabuchi and TAKEO USUI and Naoki Kanoh},
title = {Synthesis and Structure-Activity Relationship of Vicenistatin, a Cytotoxic 20-Membered Macrolactam Glycoside},
journal = {Chemistry - An Asian Journal},
year = {2012},
volume = {7},
publisher = {Wiley},
month = {sep},
url = {https://doi.org/10.1002/asia.201200615},
number = {12},
pages = {2872--2881},
doi = {10.1002/asia.201200615}
}
MLA
Cite this
MLA Copy
Fukuda, Hayato, et al. “Synthesis and Structure-Activity Relationship of Vicenistatin, a Cytotoxic 20-Membered Macrolactam Glycoside.” Chemistry - An Asian Journal, vol. 7, no. 12, Sep. 2012, pp. 2872-2881. https://doi.org/10.1002/asia.201200615.