volume 123 issue 12 pages 2267-2271

Orotate complexes. Synthesis and crystal structure of lithium orotate(—I) monohydrate and magnesium bis[ orotate(—I)] octahydrate

Publication typeJournal Article
Publication date1990-12-01
SJR
CiteScore
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ISSN00092940
Inorganic Chemistry
Abstract
Neutralization of orotic acid (OrH2) by lithium or magnesium hydroxide in aqueous medium yields the crystalline metal orotate hydrates Li(OrH). H2O (1) and Mg(OrH)2. (H2O)6 (2). By single-crystal X-ray diffraction studies it has been shown that 1 (space group P1) forms a layer structure, with lithium in a tetrahedral environment of oxygen atoms from three different orotate( - I) anions (one carboxylate and two uracil oxygen atoms) and the water molecule. 2 (space group P21/c) has been shown to feature a hexaquo complex of magnesium, the Mg(H2O)26 cations being associated with two hydrated OrH⊖ ions only through hydrogen bonds. The anions are also engaged in “base-pairing” hydrogen bonds between the planar uracil ring systems of different units. The results are relevant for applications of magnesium orotates in magnesium therapy.
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Bach I., Kumberger O., Schmidbaur H. Orotate complexes. Synthesis and crystal structure of lithium orotate(—I) monohydrate and magnesium bis[ orotate(—I)] octahydrate // Chemische Berichte. 1990. Vol. 123. No. 12. pp. 2267-2271.
GOST all authors (up to 50) Copy
Bach I., Kumberger O., Schmidbaur H. Orotate complexes. Synthesis and crystal structure of lithium orotate(—I) monohydrate and magnesium bis[ orotate(—I)] octahydrate // Chemische Berichte. 1990. Vol. 123. No. 12. pp. 2267-2271.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1002/cber.19901231207
UR - https://doi.org/10.1002/cber.19901231207
TI - Orotate complexes. Synthesis and crystal structure of lithium orotate(—I) monohydrate and magnesium bis[ orotate(—I)] octahydrate
T2 - Chemische Berichte
AU - Bach, Ina
AU - Kumberger, Otto
AU - Schmidbaur, H.
PY - 1990
DA - 1990/12/01
PB - Wiley
SP - 2267-2271
IS - 12
VL - 123
SN - 0009-2940
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{1990_Bach,
author = {Ina Bach and Otto Kumberger and H. Schmidbaur},
title = {Orotate complexes. Synthesis and crystal structure of lithium orotate(—I) monohydrate and magnesium bis[ orotate(—I)] octahydrate},
journal = {Chemische Berichte},
year = {1990},
volume = {123},
publisher = {Wiley},
month = {dec},
url = {https://doi.org/10.1002/cber.19901231207},
number = {12},
pages = {2267--2271},
doi = {10.1002/cber.19901231207}
}
MLA
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MLA Copy
Bach, Ina, et al. “Orotate complexes. Synthesis and crystal structure of lithium orotate(—I) monohydrate and magnesium bis[ orotate(—I)] octahydrate.” Chemische Berichte, vol. 123, no. 12, Dec. 1990, pp. 2267-2271. https://doi.org/10.1002/cber.19901231207.