European Journal of Organic Chemistry, volume 2019, issue 1, pages 91-94
First Synthesis of Aliphatic Nitro-NNO -azoxy Compounds
Leonov Nikita E
1
,
Klenov Michael S
1
,
Anikin Oleg V
1
,
Strelenko Yurii A.
1
,
Tartakovsky Vladimir A
1
Publication type: Journal Article
Publication date: 2018-12-10
Quartile SCImago
Q2
Quartile WOS
Q2
Impact factor: 2.8
ISSN: 1434193X, 10990690
Organic Chemistry
Physical and Theoretical Chemistry
Abstract
The first aliphatic nitro‐NNO‐azoxy compounds were synthesized by substitutive nitration of appropriate tert‐butyl‐NNO‐azoxy compounds with nitronium tetrafluoroborate. Nitro(nitro‐NNO‐azoxy)methane (1), (tert‐butyl‐NNO‐azoxy)(nitro‐NNO‐azoxy)methane (2), bis(nitro‐NNO‐azoxy)methane (3), and 2‐nitro‐2‐(nitro‐NNO‐azoxy)propane (4) were prepared. Compound 4 with the nitro‐NNO‐azoxy group bound with the tertiary C atom appeared most stable (DSC, onset temperature of decomposition 104 °C). Compound 2 was less stable (DSC, onset temperature 88 °C). Compounds with strong electron withdrawing substituents had the least stability, assumingly, due to rather high acidity of CH protons alongside with instability of C‐anions of nitro‐NNO‐azoxy compounds.
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- We do not take into account publications that without a DOI.
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Leonov N. E. et al. First Synthesis of Aliphatic Nitro-NNO -azoxy Compounds // European Journal of Organic Chemistry. 2018. Vol. 2019. No. 1. pp. 91-94.
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Leonov N. E., Klenov M. S., Anikin O. V., Churakov A. M., Strelenko Y. A., Monogarov K., Tartakovsky V. A. First Synthesis of Aliphatic Nitro-NNO -azoxy Compounds // European Journal of Organic Chemistry. 2018. Vol. 2019. No. 1. pp. 91-94.
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TY - JOUR
DO - 10.1002/ejoc.201801533
UR - https://doi.org/10.1002%2Fejoc.201801533
TI - First Synthesis of Aliphatic Nitro-NNO -azoxy Compounds
T2 - European Journal of Organic Chemistry
AU - Leonov, Nikita E
AU - Klenov, Michael S
AU - Anikin, Oleg V
AU - Strelenko, Yurii A.
AU - Tartakovsky, Vladimir A
AU - Churakov, Aleksandr M
AU - Monogarov, Konstantin
PY - 2018
DA - 2018/12/10 00:00:00
PB - Wiley
SP - 91-94
IS - 1
VL - 2019
SN - 1434-193X
SN - 1099-0690
ER -
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@article{2018_Leonov,
author = {Nikita E Leonov and Michael S Klenov and Oleg V Anikin and Yurii A. Strelenko and Vladimir A Tartakovsky and Aleksandr M Churakov and Konstantin Monogarov},
title = {First Synthesis of Aliphatic Nitro-NNO -azoxy Compounds},
journal = {European Journal of Organic Chemistry},
year = {2018},
volume = {2019},
publisher = {Wiley},
month = {dec},
url = {https://doi.org/10.1002%2Fejoc.201801533},
number = {1},
pages = {91--94},
doi = {10.1002/ejoc.201801533}
}
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MLA
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Leonov, Nikita E., et al. “First Synthesis of Aliphatic Nitro-NNO -azoxy Compounds.” European Journal of Organic Chemistry, vol. 2019, no. 1, Dec. 2018, pp. 91-94. https://doi.org/10.1002%2Fejoc.201801533.
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