Preparation ofC2-Symmetric Bis[2-(diphenylphosphino)ferrocen-1-yl]- methane and Its Use in Rhodium- and Ruthenium-Catalyzed Hydrogenation
2
Institute of Chemical Technologies and Analytics, Vienna University of Technology, Getreidemarkt 9, A-1060 Vienna
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3
Solvias AG, WKL 127, P. O. Box, CH‐4002 Basel
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Тип публикации: Journal Article
Дата публикации: 2006-08-30
scimago Q2
wos Q3
БС2
SJR: 0.491
CiteScore: 3.0
Impact factor: 1.8
ISSN: 0018019X, 15222675
Catalysis
Organic Chemistry
Drug Discovery
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
The two diphosphine ligands (Rp,Rp)- and (Sp,Sp)-bis[2-(diphenylphospino)ferrocenyl]methane, (Rp,Rp)- and (Sp,Sp)-1, resp., were prepared in six steps from (S)- and (R)-ferrocenyl tolyl sulfoxide, respectively (Scheme). In the solid state, both the diborane complex (Rp,Rp)-1 ⋅ (BH3)2 and the palladium dichloride complex [PdCl2((Rp,Rp)-1)] were found to adopt C2-pseudosymmetric structures according to X-ray analyses (Figs. 2 and 3). In the Rh- and Ru-catalyzed hydrogenation of selected alkenes and ketones in the presence of the new ligands, enantioselectivities of up to 55% ee were obtained.
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Wang Y. et al. Preparation ofC2-Symmetric Bis[2-(diphenylphosphino)ferrocen-1-yl]- methane and Its Use in Rhodium- and Ruthenium-Catalyzed Hydrogenation // Helvetica Chimica Acta. 2006. Vol. 89. No. 8. pp. 1772-1782.
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Wang Y., Weissensteiner W., Mereiter K., Spindler F. Preparation ofC2-Symmetric Bis[2-(diphenylphosphino)ferrocen-1-yl]- methane and Its Use in Rhodium- and Ruthenium-Catalyzed Hydrogenation // Helvetica Chimica Acta. 2006. Vol. 89. No. 8. pp. 1772-1782.
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TY - JOUR
DO - 10.1002/hlca.200690173
UR - https://doi.org/10.1002/hlca.200690173
TI - Preparation ofC2-Symmetric Bis[2-(diphenylphosphino)ferrocen-1-yl]- methane and Its Use in Rhodium- and Ruthenium-Catalyzed Hydrogenation
T2 - Helvetica Chimica Acta
AU - Wang, Yaping
AU - Weissensteiner, Walter
AU - Mereiter, K.
AU - Spindler, Felix
PY - 2006
DA - 2006/08/30
PB - Wiley
SP - 1772-1782
IS - 8
VL - 89
SN - 0018-019X
SN - 1522-2675
ER -
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@article{2006_Wang,
author = {Yaping Wang and Walter Weissensteiner and K. Mereiter and Felix Spindler},
title = {Preparation ofC2-Symmetric Bis[2-(diphenylphosphino)ferrocen-1-yl]- methane and Its Use in Rhodium- and Ruthenium-Catalyzed Hydrogenation},
journal = {Helvetica Chimica Acta},
year = {2006},
volume = {89},
publisher = {Wiley},
month = {aug},
url = {https://doi.org/10.1002/hlca.200690173},
number = {8},
pages = {1772--1782},
doi = {10.1002/hlca.200690173}
}
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Wang, Yaping, et al. “Preparation ofC2-Symmetric Bis[2-(diphenylphosphino)ferrocen-1-yl]- methane and Its Use in Rhodium- and Ruthenium-Catalyzed Hydrogenation.” Helvetica Chimica Acta, vol. 89, no. 8, Aug. 2006, pp. 1772-1782. https://doi.org/10.1002/hlca.200690173.