Identification, Synthesis, and Characterization of Process Related Impurities in the Synthesis of Boc‐L‐Lys(Boc)‐OSu
1
Department of Synthetic Chemistry Embio Research Centre, Embio Limited Raigad India
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Publication type: Journal Article
Publication date: 2024-09-12
scimago Q3
wos Q2
SJR: 0.362
CiteScore: 4.7
Impact factor: 2.4
ISSN: 0022152X, 19435193
Abstract
ABSTRACT
Protected lysine esters (Boc‐L‐Lys(Boc)‐OSu) an intermediate of high repute in the peptide synthesis and diverse chemical synthetic applications, was the subject of synthetic process development studies, unveiling process‐related impurities. These impurities were synthesized, characterized, and identified by different analytical tools, with their retention times verified by HPLC co‐injection with commercial products. Detailed discussions ensued on the potential formation pathways and synthetic strategies of these process‐related impurities.
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Pakhurde A., Kishore D., Kotharkar S. A. Identification, Synthesis, and Characterization of Process Related Impurities in the Synthesis of Boc‐L‐Lys(Boc)‐OSu // Journal of Heterocyclic Chemistry. 2024. Vol. 61. No. 11. pp. 1710-1720.
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Pakhurde A., Kishore D., Kotharkar S. A. Identification, Synthesis, and Characterization of Process Related Impurities in the Synthesis of Boc‐L‐Lys(Boc)‐OSu // Journal of Heterocyclic Chemistry. 2024. Vol. 61. No. 11. pp. 1710-1720.
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TY - JOUR
DO - 10.1002/jhet.4884
UR - https://onlinelibrary.wiley.com/doi/10.1002/jhet.4884
TI - Identification, Synthesis, and Characterization of Process Related Impurities in the Synthesis of Boc‐L‐Lys(Boc)‐OSu
T2 - Journal of Heterocyclic Chemistry
AU - Pakhurde, Amit H.
AU - Kishore, D. V. P.
AU - Kotharkar, Sandeep A
PY - 2024
DA - 2024/09/12
PB - Wiley
SP - 1710-1720
IS - 11
VL - 61
SN - 0022-152X
SN - 1943-5193
ER -
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BibTex (up to 50 authors)
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@article{2024_Pakhurde,
author = {Amit H. Pakhurde and D. V. P. Kishore and Sandeep A Kotharkar},
title = {Identification, Synthesis, and Characterization of Process Related Impurities in the Synthesis of Boc‐L‐Lys(Boc)‐OSu},
journal = {Journal of Heterocyclic Chemistry},
year = {2024},
volume = {61},
publisher = {Wiley},
month = {sep},
url = {https://onlinelibrary.wiley.com/doi/10.1002/jhet.4884},
number = {11},
pages = {1710--1720},
doi = {10.1002/jhet.4884}
}
Cite this
MLA
Copy
Pakhurde, Amit H., et al. “Identification, Synthesis, and Characterization of Process Related Impurities in the Synthesis of Boc‐L‐Lys(Boc)‐OSu.” Journal of Heterocyclic Chemistry, vol. 61, no. 11, Sep. 2024, pp. 1710-1720. https://onlinelibrary.wiley.com/doi/10.1002/jhet.4884.