Mannich reaction on 2-(2-benzofuranyl)-1H-indole. Determination of structure by NMR spectroscopic techniques
1
Chemistry Research Department, Pharmaceutical Division, Sandoz, Inc., East Hanover, New Jersey 07936
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Publication type: Journal Article
Publication date: 1981-05-01
scimago Q3
wos Q2
SJR: 0.362
CiteScore: 4.7
Impact factor: 2.4
ISSN: 0022152X, 19435193
Organic Chemistry
Abstract
Analysis of the product from the Mannich reaction of 2-(2-benzofuranyl)-1H-indole via 1H and 13C nmr spectroscopy was performed. The studies included use of Pr(Fod)3 shift reagent, proton-coupled 13C spectra, deuterium isotope induced shifts and protonation studies. It was found that the reaction occurred on the indole moiety at C-3.
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Badger E. et al. Mannich reaction on 2-(2-benzofuranyl)-1H-indole. Determination of structure by NMR spectroscopic techniques // Journal of Heterocyclic Chemistry. 1981. Vol. 18. No. 3. pp. 623-626.
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Badger E., Dicataldo S., Kahle A. D., Nadelson J., Shapiro M. J. Mannich reaction on 2-(2-benzofuranyl)-1H-indole. Determination of structure by NMR spectroscopic techniques // Journal of Heterocyclic Chemistry. 1981. Vol. 18. No. 3. pp. 623-626.
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TY - JOUR
DO - 10.1002/jhet.5570180337
UR - https://doi.org/10.1002/jhet.5570180337
TI - Mannich reaction on 2-(2-benzofuranyl)-1H-indole. Determination of structure by NMR spectroscopic techniques
T2 - Journal of Heterocyclic Chemistry
AU - Badger, E
AU - Dicataldo, S
AU - Kahle, A D
AU - Nadelson, J
AU - Shapiro, M. J.
PY - 1981
DA - 1981/05/01
PB - Wiley
SP - 623-626
IS - 3
VL - 18
SN - 0022-152X
SN - 1943-5193
ER -
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BibTex (up to 50 authors)
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@article{1981_Badger,
author = {E Badger and S Dicataldo and A D Kahle and J Nadelson and M. J. Shapiro},
title = {Mannich reaction on 2-(2-benzofuranyl)-1H-indole. Determination of structure by NMR spectroscopic techniques},
journal = {Journal of Heterocyclic Chemistry},
year = {1981},
volume = {18},
publisher = {Wiley},
month = {may},
url = {https://doi.org/10.1002/jhet.5570180337},
number = {3},
pages = {623--626},
doi = {10.1002/jhet.5570180337}
}
Cite this
MLA
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Badger, E., et al. “Mannich reaction on 2-(2-benzofuranyl)-1H-indole. Determination of structure by NMR spectroscopic techniques.” Journal of Heterocyclic Chemistry, vol. 18, no. 3, May. 1981, pp. 623-626. https://doi.org/10.1002/jhet.5570180337.