Synthesis of hexadeuterated hexestrol (R, S)-3,4-di-(4-hydroxyphenyl)hexane-1,1,1,6,6,6-2H6
Publication type: Journal Article
Publication date: 1985-10-01
scimago Q3
wos Q4
SJR: 0.271
CiteScore: 2.0
Impact factor: 0.9
ISSN: 03624803, 10991344
Organic Chemistry
Drug Discovery
Biochemistry
Spectroscopy
Analytical Chemistry
Radiology, Nuclear Medicine and imaging
Abstract
A short and stereoselective synthesis of hexadeuterated hexestrol is described, involving catalytic hydrogenation of Z-3,4-di-(4-methoxyphenyl)hex-3-ene-1,1,1,6,6,6-2H6 followed by demethylation using sodium thioethoxide in dimethyl formamide.
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De Clercq P. J. et al. Synthesis of hexadeuterated hexestrol (R, S)-3,4-di-(4-hydroxyphenyl)hexane-1,1,1,6,6,6-2H6 // Journal of Labelled Compounds and Radiopharmaceuticals. 1985. Vol. 22. No. 10. pp. 1087-1091.
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De Clercq P. J., Hoflack J. M., Van Royen L. A., Van Peteghem C. H. Synthesis of hexadeuterated hexestrol (R, S)-3,4-di-(4-hydroxyphenyl)hexane-1,1,1,6,6,6-2H6 // Journal of Labelled Compounds and Radiopharmaceuticals. 1985. Vol. 22. No. 10. pp. 1087-1091.
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TY - JOUR
DO - 10.1002/jlcr.2580221012
UR - https://doi.org/10.1002/jlcr.2580221012
TI - Synthesis of hexadeuterated hexestrol (R, S)-3,4-di-(4-hydroxyphenyl)hexane-1,1,1,6,6,6-2H6
T2 - Journal of Labelled Compounds and Radiopharmaceuticals
AU - De Clercq, P J
AU - Hoflack, J M
AU - Van Royen, L A
AU - Van Peteghem, C H
PY - 1985
DA - 1985/10/01
PB - Wiley
SP - 1087-1091
IS - 10
VL - 22
SN - 0362-4803
SN - 1099-1344
ER -
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@article{1985_De Clercq,
author = {P J De Clercq and J M Hoflack and L A Van Royen and C H Van Peteghem},
title = {Synthesis of hexadeuterated hexestrol (R, S)-3,4-di-(4-hydroxyphenyl)hexane-1,1,1,6,6,6-2H6},
journal = {Journal of Labelled Compounds and Radiopharmaceuticals},
year = {1985},
volume = {22},
publisher = {Wiley},
month = {oct},
url = {https://doi.org/10.1002/jlcr.2580221012},
number = {10},
pages = {1087--1091},
doi = {10.1002/jlcr.2580221012}
}
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De Clercq, P. J., et al. “Synthesis of hexadeuterated hexestrol (R, S)-3,4-di-(4-hydroxyphenyl)hexane-1,1,1,6,6,6-2H6.” Journal of Labelled Compounds and Radiopharmaceuticals, vol. 22, no. 10, Oct. 1985, pp. 1087-1091. https://doi.org/10.1002/jlcr.2580221012.