volume 63 issue 1 pages 74-77

Hydrolysis of Steroid Oximes: Mechanism and Products

Richard E Huettemann 1
Arvin P Shroff 1
1
 
Analytical Research Group, Division of Chemical Research, Ortho Research Foundation, Raritan, NJ 08869
Publication typeJournal Article
Publication date1974-01-01
scimago Q1
wos Q2
SJR0.737
CiteScore7.2
Impact factor3.8
ISSN00223549, 15206017
Pharmaceutical Science
Abstract
The conversion of 17α-acetoxy-6αmethyl-4-pregnen-3,20-dione 3-oxime to the corresponding diketone in acidic media was found to be a first-order reaction at 37°. The effects of incorporating ester groupings at the oxime function or at the C-17 position and modifications in ring B were also investigated. Only the length of the ester chain at the oxime function had a profound effect on the rate constant. From these observations, it is proposed that two competing mechanisms of hydrolysis are involved for the oxime esters.
Found 
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Huettemann R. E., Shroff A. P. Hydrolysis of Steroid Oximes: Mechanism and Products // Journal of Pharmaceutical Sciences. 1974. Vol. 63. No. 1. pp. 74-77.
GOST all authors (up to 50) Copy
Huettemann R. E., Shroff A. P. Hydrolysis of Steroid Oximes: Mechanism and Products // Journal of Pharmaceutical Sciences. 1974. Vol. 63. No. 1. pp. 74-77.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1002/jps.2600630118
UR - https://doi.org/10.1002/jps.2600630118
TI - Hydrolysis of Steroid Oximes: Mechanism and Products
T2 - Journal of Pharmaceutical Sciences
AU - Huettemann, Richard E
AU - Shroff, Arvin P
PY - 1974
DA - 1974/01/01
PB - Elsevier
SP - 74-77
IS - 1
VL - 63
PMID - 4811289
SN - 0022-3549
SN - 1520-6017
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{1974_Huettemann,
author = {Richard E Huettemann and Arvin P Shroff},
title = {Hydrolysis of Steroid Oximes: Mechanism and Products},
journal = {Journal of Pharmaceutical Sciences},
year = {1974},
volume = {63},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1002/jps.2600630118},
number = {1},
pages = {74--77},
doi = {10.1002/jps.2600630118}
}
MLA
Cite this
MLA Copy
Huettemann, Richard E., and Arvin P Shroff. “Hydrolysis of Steroid Oximes: Mechanism and Products.” Journal of Pharmaceutical Sciences, vol. 63, no. 1, Jan. 1974, pp. 74-77. https://doi.org/10.1002/jps.2600630118.