volume 9 issue 8

Synthesis of 1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one and analysis of its structure by X‐ray crystallography, NMR, UV‐Vis spectroscopy and DFT calculations

M Yu Volkov 1
Alsu R Sharipova 1
O A Turanova 1
Aidar T Gubaidullin 2
Amina F Shaidullina 3
Alexander N Turanov 1
Publication typeJournal Article
Publication date2024-02-21
scimago Q3
wos Q3
SJR0.366
CiteScore3.0
Impact factor2.0
ISSN23656549
General Chemistry
Abstract

1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one was obtained by a two‐step synthesis. From X‐ray crystallography, NMR and UV‐vis spectra it follows that in the crystalline state and in solutions, regardless of the polarity of the solvent, 1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one exists in the ketone form of the cis‐isomer. DFT calculations confirmed that the cis‐isomer is the most energetically favorable among all its isomers.

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Volkov M. Yu. et al. Synthesis of 1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one and analysis of its structure by X‐ray crystallography, NMR, UV‐Vis spectroscopy and DFT calculations // ChemistrySelect. 2024. Vol. 9. No. 8.
GOST all authors (up to 50) Copy
Volkov M. Yu., Sharipova A. R., Turanova O. A., Gubaidullin A. T., Shaidullina A. F., Savostina L. I., Turanov A. N. Synthesis of 1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one and analysis of its structure by X‐ray crystallography, NMR, UV‐Vis spectroscopy and DFT calculations // ChemistrySelect. 2024. Vol. 9. No. 8.
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TY - JOUR
DO - 10.1002/slct.202304190
UR - https://doi.org/10.1002/slct.202304190
TI - Synthesis of 1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one and analysis of its structure by X‐ray crystallography, NMR, UV‐Vis spectroscopy and DFT calculations
T2 - ChemistrySelect
AU - Volkov, M Yu
AU - Sharipova, Alsu R
AU - Turanova, O A
AU - Gubaidullin, Aidar T
AU - Shaidullina, Amina F
AU - Savostina, Ludmila I.
AU - Turanov, Alexander N
PY - 2024
DA - 2024/02/21
PB - Wiley
IS - 8
VL - 9
SN - 2365-6549
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2024_Volkov,
author = {M Yu Volkov and Alsu R Sharipova and O A Turanova and Aidar T Gubaidullin and Amina F Shaidullina and Ludmila I. Savostina and Alexander N Turanov},
title = {Synthesis of 1‐phenyl‐3‐(quinolin‐8‐ylamino)prop‐2‐en‐1‐one and analysis of its structure by X‐ray crystallography, NMR, UV‐Vis spectroscopy and DFT calculations},
journal = {ChemistrySelect},
year = {2024},
volume = {9},
publisher = {Wiley},
month = {feb},
url = {https://doi.org/10.1002/slct.202304190},
number = {8},
doi = {10.1002/slct.202304190}
}