том 29 , издание 2 , страницы 197-198

Bis(1,4,7-trithiacyclononane)gold Dication: A Paramagnetic, Mononuclear AuII Complex

Тип публикации: Journal Article

Дата публикации: 1990-02-01

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DOI: 10.1002/anie.199001971

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General Chemistry

Catalysis

Краткое описание

The d9 AuII complex 1 is unambiguously mono-nuclear. It was obtained by reaction of KAuCl4 with two equivalents of 1,4,7-trithiacyclononane ([9]aneS3) in refluxing aqueous HBF4/MeOH (structure of [Au([9]aneS3)2]2⊕, 1, at the right). The ESR spectrum shows a strong signal at g = 2.010 (T = 77K) displaying clear hyperfine coupling. A delocalization of the positive charge of 1 over the ligands is presumably of only minor importance.

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