DOSY Analysis of Micromolar Analytes: Resolving Dilute Mixtures by SABRE Hyperpolarization
Indrek Reile
1
,
Ruud L. E. G. Aspers
1
,
Jean Max Tyburn
2
,
J. G. Kempf
3
,
Martin Feiters
1
,
Floris P. J. T. Rutjes
1
,
M. Tessari
1
2
Bruker BioSpin GmbH; Silberstreifen Rheinstetten Germany
|
3
Bruker Biospin Corp.; Billerica MA 01821 USA
|
Publication type: Journal Article
Publication date: 2017-06-28
scimago Q1
wos Q1
SJR: 5.550
CiteScore: 27.6
Impact factor: 16.9
ISSN: 14337851, 15213773
PubMed ID:
28590559
General Chemistry
Catalysis
Abstract
DOSY is an NMR spectroscopy technique that resolves resonances according to the analytes' diffusion coefficients. It has found use in correlating NMR signals and estimating the number of components in mixtures. Applications of DOSY in dilute mixtures are, however, held back by excessively long measurement times. We demonstrate herein, how the enhanced NMR sensitivity provided by SABRE hyperpolarization allows DOSY analysis of low-micromolar mixtures, thus reducing the concentration requirements by at least 100-fold.
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Total citations:
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Citations from 2025:
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(3.85%)
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GOST
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Reile I. et al. DOSY Analysis of Micromolar Analytes: Resolving Dilute Mixtures by SABRE Hyperpolarization // Angewandte Chemie - International Edition. 2017. Vol. 56. No. 31. pp. 9174-9177.
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Reile I., Aspers R. L. E. G., Tyburn J. M., Kempf J. G., Feiters M., Rutjes F. P. J. T., Tessari M. DOSY Analysis of Micromolar Analytes: Resolving Dilute Mixtures by SABRE Hyperpolarization // Angewandte Chemie - International Edition. 2017. Vol. 56. No. 31. pp. 9174-9177.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1002/anie.201703577
UR - https://doi.org/10.1002/anie.201703577
TI - DOSY Analysis of Micromolar Analytes: Resolving Dilute Mixtures by SABRE Hyperpolarization
T2 - Angewandte Chemie - International Edition
AU - Reile, Indrek
AU - Aspers, Ruud L. E. G.
AU - Tyburn, Jean Max
AU - Kempf, J. G.
AU - Feiters, Martin
AU - Rutjes, Floris P. J. T.
AU - Tessari, M.
PY - 2017
DA - 2017/06/28
PB - Wiley
SP - 9174-9177
IS - 31
VL - 56
PMID - 28590559
SN - 1433-7851
SN - 1521-3773
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2017_Reile,
author = {Indrek Reile and Ruud L. E. G. Aspers and Jean Max Tyburn and J. G. Kempf and Martin Feiters and Floris P. J. T. Rutjes and M. Tessari},
title = {DOSY Analysis of Micromolar Analytes: Resolving Dilute Mixtures by SABRE Hyperpolarization},
journal = {Angewandte Chemie - International Edition},
year = {2017},
volume = {56},
publisher = {Wiley},
month = {jun},
url = {https://doi.org/10.1002/anie.201703577},
number = {31},
pages = {9174--9177},
doi = {10.1002/anie.201703577}
}
Cite this
MLA
Copy
Reile, Indrek, et al. “DOSY Analysis of Micromolar Analytes: Resolving Dilute Mixtures by SABRE Hyperpolarization.” Angewandte Chemie - International Edition, vol. 56, no. 31, Jun. 2017, pp. 9174-9177. https://doi.org/10.1002/anie.201703577.