Angewandte Chemie - International Edition

, том 57 , издание 17 , страницы 4769-4773

Me ₃ Si−SiMe ₂ [ o CON( i Pr) ₂ −C ₆ H ₄ ]: An Unsymmetrical Disilane Reagent for Regio‐ and Stereoselective Bis‐Silylation of Alkynes

Тип публикации: Journal Article

Дата публикации: 2018-03-12

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Angewandte Chemie - International Edition

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SJR: 5.495

CiteScore: 27.6

Impact factor: 16.9

ISSN: 14337851, 15213773

DOI: 10.1002/anie.201800513

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PubMed ID: 29442434

General Chemistry

Catalysis

Краткое описание

The air-stable unsymmetrical disilane Me3 Si-SiMe2 [oCON(iPr)2 C6 H4 ] has been developed for bis-silylation of alkynes. This reagent tolerates a range of functional groups, providing Z-vinyl disilanes in high yields. It is proposed that the phenyl-ring-tethered amide group directs oxidative addition of Pd0 into the Si-Si bond, which might facilitate formation of a six-membered Pd cycle, generating products with good to excellent regioselectivity.

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Xiao P. et al. Me 3 Si−SiMe 2 [ o CON( i Pr) 2 −C 6 H 4 ]: An Unsymmetrical Disilane Reagent for Regio‐ and Stereoselective Bis‐Silylation of Alkynes // Angewandte Chemie - International Edition. 2018. Vol. 57. No. 17. pp. 4769-4773.

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Xiao P., Cao Y., Gui Y., Gao L., Song Z. Me 3 Si−SiMe 2 [ o CON( i Pr) 2 −C 6 H 4 ]: An Unsymmetrical Disilane Reagent for Regio‐ and Stereoselective Bis‐Silylation of Alkynes // Angewandte Chemie - International Edition. 2018. Vol. 57. No. 17. pp. 4769-4773.

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TY - JOUR

DO - 10.1002/anie.201800513

UR - https://doi.org/10.1002/anie.201800513

TI - Me 3 Si−SiMe 2 [ o CON( i Pr) 2 −C 6 H 4 ]: An Unsymmetrical Disilane Reagent for Regio‐ and Stereoselective Bis‐Silylation of Alkynes

T2 - Angewandte Chemie - International Edition

AU - Xiao, Peihong

AU - Cao, Yanjun

AU - Gui, Yingying

AU - Gao, Lu

AU - Song, Zhenlei

PY - 2018

DA - 2018/03/12

PB - Wiley

SP - 4769-4773

IS - 17

VL - 57

PMID - 29442434

SN - 1433-7851

SN - 1521-3773

ER -

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@article{2018_Xiao,

author = {Peihong Xiao and Yanjun Cao and Yingying Gui and Lu Gao and Zhenlei Song},

title = {Me 3 Si−SiMe 2 [ o CON( i Pr) 2 −C 6 H 4 ]: An Unsymmetrical Disilane Reagent for Regio‐ and Stereoselective Bis‐Silylation of Alkynes},

journal = {Angewandte Chemie - International Edition},

year = {2018},

volume = {57},

publisher = {Wiley},

month = {mar},

url = {https://doi.org/10.1002/anie.201800513},

number = {17},

pages = {4769--4773},

doi = {10.1002/anie.201800513}

}

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Xiao, Peihong, et al. “Me 3 Si−SiMe 2 [ o CON( i Pr) 2 −C 6 H 4 ]: An Unsymmetrical Disilane Reagent for Regio‐ and Stereoselective Bis‐Silylation of Alkynes.” Angewandte Chemie - International Edition, vol. 57, no. 17, Mar. 2018, pp. 4769-4773. https://doi.org/10.1002/anie.201800513.

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Angewandte Chemie - International Edition

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