Rhodium(I) carbonyl complexes of ether-phosphine ligands and their reactivity
Тип публикации: Journal Article
Дата публикации: 2002-08-25
scimago Q2
БС1
SJR: 0.515
CiteScore: 6.5
Impact factor: 3.7
ISSN: 02682605, 10990739
General Chemistry
Inorganic Chemistry
Краткое описание
The reactions of dimeric complex [Rh(CO) 2 Cl] 2 with hemilabile ether-phosphine ligands Ph 2 P(CH 2 ) n OR [n = 1, R = CH 3 (a); n = 2, R = C 2 H 5 (b)] yield cis-[Rh(CO) 2 Cl(P∼O)] (1) [P ∼ O = η 1 -(P) coordinated]. Halide abstraction reactions of 1 with AgClO 4 produce cis-[Rh(CO) 2 (P n O)]ClO 4 (2) [P ∩ O = η 2 -(P,O)chelated]. Oxidative addition reactions of 1 with CH 3 I and I 2 give rhodium(III) complexes [Rh(CO)(COCH 3 )ClI(P ∩ O)] (3) and [Rh(CO)ClI 2 (P ∩ O)] (4) respectively. The complexes have been characterized by elemental analyses, IR, 1 H, 13 C and 31 P NMR spectroscopy. The catalytic activity of 1 for carbonylation of methanol is higher than that of the well-known [Rh(CO) 2 I 2 ] - species.
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ГОСТ
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Das P. et al. Rhodium(I) carbonyl complexes of ether-phosphine ligands and their reactivity // Applied Organometallic Chemistry. 2002. Vol. 16. No. 6. pp. 302-306.
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Das P., Sharma M., Kumari N., Konwar D., Dutta D. Rhodium(I) carbonyl complexes of ether-phosphine ligands and their reactivity // Applied Organometallic Chemistry. 2002. Vol. 16. No. 6. pp. 302-306.
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TY - JOUR
DO - 10.1002/aoc.300
UR - https://doi.org/10.1002/aoc.300
TI - Rhodium(I) carbonyl complexes of ether-phosphine ligands and their reactivity
T2 - Applied Organometallic Chemistry
AU - Das, Pankaj
AU - Sharma, Manab
AU - Kumari, Nandini
AU - Konwar, Dilip
AU - Dutta, Dipak
PY - 2002
DA - 2002/08/25
PB - Wiley
SP - 302-306
IS - 6
VL - 16
SN - 0268-2605
SN - 1099-0739
ER -
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BibTex (до 50 авторов)
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@article{2002_Das,
author = {Pankaj Das and Manab Sharma and Nandini Kumari and Dilip Konwar and Dipak Dutta},
title = {Rhodium(I) carbonyl complexes of ether-phosphine ligands and their reactivity},
journal = {Applied Organometallic Chemistry},
year = {2002},
volume = {16},
publisher = {Wiley},
month = {aug},
url = {https://doi.org/10.1002/aoc.300},
number = {6},
pages = {302--306},
doi = {10.1002/aoc.300}
}
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MLA
Скопировать
Das, Pankaj, et al. “Rhodium(I) carbonyl complexes of ether-phosphine ligands and their reactivity.” Applied Organometallic Chemistry, vol. 16, no. 6, Aug. 2002, pp. 302-306. https://doi.org/10.1002/aoc.300.