The effect of TIBA on metallocene/MAO catalyzed synthesis of propylene oxazoline copolymers and their use in reactive blending
Publication type: Journal Article
Publication date: 2002-09-19
scimago Q2
wos Q3
SJR: 0.572
CiteScore: 5.8
Impact factor: 2.8
ISSN: 00218995, 10974628
Materials Chemistry
Surfaces, Coatings and Films
General Chemistry
Polymers and Plastics
Abstract
Oxazoline-functionalized polypropylenes were synthesized by using the rac-Et[1-Ind]2ZrCl2/MAO catalyst system. The used comonomers were 2-(9-decene-1-yl)-1,3-oxazoline (R-Ox1), 2-(9-decene-1-yl)-4,4-dimethyl-1,3-oxazoline (R-Ox2), and 2-(4-(10-undecene-1-oxy)phenyl)-1,3-oxazoline (R-Ox3). The oxazolines reduce the catalyst activity in the order R-Ox3 > R-Ox1 > R-Ox2. By the addition of triisobutylaluminum (TIBA), the catalyst poisoning is reduced and is most pronounced in the R-Ox1- and R-Ox2-containing systems. The oxazoline-containing copolymers were melt blended with carboxylic acid end-functionalized polystyrene (PS-COOH) at 200°C. Strong changes in the morphology of the reactive blends compared to the nonreactive blends, especially the cocontinuous morphology in a poly(propylene-co-R-Ox3)/PS-COOH blend, indicate the usefulness of the modified copolymers in the reactive blending processes. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 2174–2181, 2002
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Kaya A. et al. The effect of TIBA on metallocene/MAO catalyzed synthesis of propylene oxazoline copolymers and their use in reactive blending // Journal of Applied Polymer Science. 2002. Vol. 86. No. 9. pp. 2174-2181.
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Kaya A., Pompe G., Schulze U., Voit B., Pionteck J. The effect of TIBA on metallocene/MAO catalyzed synthesis of propylene oxazoline copolymers and their use in reactive blending // Journal of Applied Polymer Science. 2002. Vol. 86. No. 9. pp. 2174-2181.
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TY - JOUR
DO - 10.1002/app.11161
UR - https://doi.org/10.1002/app.11161
TI - The effect of TIBA on metallocene/MAO catalyzed synthesis of propylene oxazoline copolymers and their use in reactive blending
T2 - Journal of Applied Polymer Science
AU - Kaya, Atila
AU - Pompe, Gisela
AU - Schulze, Ulrich
AU - Voit, B.
AU - Pionteck, Jürgen
PY - 2002
DA - 2002/09/19
PB - Wiley
SP - 2174-2181
IS - 9
VL - 86
SN - 0021-8995
SN - 1097-4628
ER -
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@article{2002_Kaya,
author = {Atila Kaya and Gisela Pompe and Ulrich Schulze and B. Voit and Jürgen Pionteck},
title = {The effect of TIBA on metallocene/MAO catalyzed synthesis of propylene oxazoline copolymers and their use in reactive blending},
journal = {Journal of Applied Polymer Science},
year = {2002},
volume = {86},
publisher = {Wiley},
month = {sep},
url = {https://doi.org/10.1002/app.11161},
number = {9},
pages = {2174--2181},
doi = {10.1002/app.11161}
}
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MLA
Copy
Kaya, Atila, et al. “The effect of TIBA on metallocene/MAO catalyzed synthesis of propylene oxazoline copolymers and their use in reactive blending.” Journal of Applied Polymer Science, vol. 86, no. 9, Sep. 2002, pp. 2174-2181. https://doi.org/10.1002/app.11161.