Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill.
Publication type: Journal Article
Publication date: 2015-10-22
scimago Q1
wos Q2
SJR: 0.981
CiteScore: 6.7
Impact factor: 3.7
ISSN: 09476539, 15213765
PubMed ID:
26489706
General Chemistry
Catalysis
Organic Chemistry
Abstract
The absence of solvent, associated with intensive mechanical agitation, allowed the first mechanosynthesis of high-value silver(I)-carbene complexes and the corresponding N,N-dialkylimidazolium precursors. This procedure gave outstanding results in terms of yield and reaction time, when compared to solution-based conditions previously described in literature, and was generalized to unprecedented compounds. Silver(I)-carbene complexes could either be obtained from N,N-dialkylimidazolium salts or directly from imidazole and alkyl halides in a one-pot two-step procedure without isolating the imidazolium intermediate. Additionally, an efficient one-pot three-step sequence, including imidazole alkylation, silver metalation, and transmetalation is reported.
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Metrics
53
Total citations:
53
Citations from 2025:
7
(13.21%)
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GOST
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Beillard A. et al. Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill. // Chemistry - A European Journal. 2015. Vol. 21. No. 49. pp. 17614-17617.
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Beillard A., Golliard E., Gillet V., Bantreil X., Métro T. X., Martinez J., Lamaty F. Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill. // Chemistry - A European Journal. 2015. Vol. 21. No. 49. pp. 17614-17617.
Cite this
RIS
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TY - JOUR
DO - 10.1002/chem.201503472
UR - https://doi.org/10.1002/chem.201503472
TI - Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill.
T2 - Chemistry - A European Journal
AU - Beillard, Audrey
AU - Golliard, Ethan
AU - Gillet, Valentin
AU - Bantreil, Xavier
AU - Métro, Thomas Xavier
AU - Martinez, Jean
AU - Lamaty, Frédéric
PY - 2015
DA - 2015/10/22
PB - Wiley
SP - 17614-17617
IS - 49
VL - 21
PMID - 26489706
SN - 0947-6539
SN - 1521-3765
ER -
Cite this
BibTex (up to 50 authors)
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@article{2015_Beillard,
author = {Audrey Beillard and Ethan Golliard and Valentin Gillet and Xavier Bantreil and Thomas Xavier Métro and Jean Martinez and Frédéric Lamaty},
title = {Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill.},
journal = {Chemistry - A European Journal},
year = {2015},
volume = {21},
publisher = {Wiley},
month = {oct},
url = {https://doi.org/10.1002/chem.201503472},
number = {49},
pages = {17614--17617},
doi = {10.1002/chem.201503472}
}
Cite this
MLA
Copy
Beillard, Audrey, et al. “Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill..” Chemistry - A European Journal, vol. 21, no. 49, Oct. 2015, pp. 17614-17617. https://doi.org/10.1002/chem.201503472.