Direct Synthesis of 3‐Aryl Substituted Isocoumarins and Phthalides through Palladium Acetate Catalyzed C( sp 2 )−H Activation in Ionic Liquids
Andrea Aloia
1
,
Michele Casiello
1
,
Lucia D’Accolti
1, 2
,
Caterina Fusco
2
,
Angelo Nacci
1, 2
,
Antonio Monopoli
1, 2
Publication type: Journal Article
Publication date: 2022-09-19
scimago Q1
wos Q2
SJR: 0.981
CiteScore: 6.7
Impact factor: 3.7
ISSN: 09476539, 15213765
PubMed ID:
35997238
General Chemistry
Catalysis
Organic Chemistry
Abstract
A novel Pd-catalysed oxidative coupling between benzoic acids and vinylarenes or acrylates to furnish isocoumarins and phthalides is reported. The reaction proceeds smoothly in molten tetrabutylammonium acetate via a selective C-H bond activation, with very low percentage of ligand-free palladium acetate as the catalyst, under atmospheric pressure of oxygen. Sub-stoichiometric amount of copper acetate is also required as a reoxidant for the palladium.
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Metrics
13
Total citations:
13
Citations from 2024:
9
(69.23%)
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GOST
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Aloia A. et al. Direct Synthesis of 3‐Aryl Substituted Isocoumarins and Phthalides through Palladium Acetate Catalyzed C( sp 2 )−H Activation in Ionic Liquids // Chemistry - A European Journal. 2022. Vol. 28. No. 65.
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Aloia A., Casiello M., D’Accolti L., Fusco C., Nacci A., Monopoli A. Direct Synthesis of 3‐Aryl Substituted Isocoumarins and Phthalides through Palladium Acetate Catalyzed C( sp 2 )−H Activation in Ionic Liquids // Chemistry - A European Journal. 2022. Vol. 28. No. 65.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1002/chem.202202350
UR - https://doi.org/10.1002/chem.202202350
TI - Direct Synthesis of 3‐Aryl Substituted Isocoumarins and Phthalides through Palladium Acetate Catalyzed C( sp 2 )−H Activation in Ionic Liquids
T2 - Chemistry - A European Journal
AU - Aloia, Andrea
AU - Casiello, Michele
AU - D’Accolti, Lucia
AU - Fusco, Caterina
AU - Nacci, Angelo
AU - Monopoli, Antonio
PY - 2022
DA - 2022/09/19
PB - Wiley
IS - 65
VL - 28
PMID - 35997238
SN - 0947-6539
SN - 1521-3765
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2022_Aloia,
author = {Andrea Aloia and Michele Casiello and Lucia D’Accolti and Caterina Fusco and Angelo Nacci and Antonio Monopoli},
title = {Direct Synthesis of 3‐Aryl Substituted Isocoumarins and Phthalides through Palladium Acetate Catalyzed C( sp 2 )−H Activation in Ionic Liquids},
journal = {Chemistry - A European Journal},
year = {2022},
volume = {28},
publisher = {Wiley},
month = {sep},
url = {https://doi.org/10.1002/chem.202202350},
number = {65},
doi = {10.1002/chem.202202350}
}