European Journal of Inorganic Chemistry

, том 2004 , издание 10 , страницы 2123-2129

Reaction of [In(NEt2)3]2 with N(CH 2CH2NSiMe3H)3: Synthesis and characterization of new azaindatranes and azaindocane

Pavel L Shutov ¹

Sergey S. Karlov ²

K. Harms ¹

Andrei V. Churakov ³

Jörg Lorberth ¹

Galina S. Zaitseva ²

Скрыть аффилиации авторов Показать аффилиации авторов: 3 аффилиации

Fachbereich Chemie, Philipps‐Universität Marburg, Hans‐Meerwein‐Strasse, 35032 Marburg/Lahn, Germany |

Chemistry Department, Moscow State University, Leninskie Gory 1, str. 3, 119899 Moscow, Russia |

Institute of General and Inorganic Chemistry, RAS, Leninsky Prospect 31, 119991 Moscow, Russia |

Тип публикации: Journal Article

Дата публикации: 2004-05-01

Wiley

European Journal of Inorganic Chemistry

scimago Q2

wos Q3

БС2

SJR: 0.459

CiteScore: 3.9

Impact factor: 2.0

ISSN: 14341948, 10990682

DOI: 10.1002/ejic.200300875

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Inorganic Chemistry

Краткое описание

[In(NEt₂)₃]₂ and N(CH₂CH₂NSiMe₃H)₃ react to yield monomeric azaindatrane 1, N(CH₂CH₂NSiMe₃)₃In, which is unstable without additional donor (e.g. pyridine), turning into dimeric azaindatrane 2, [N(CH₂CH₂NSiMe₃)₂(CH₂CH₂NH)In]₂. An intermediate product of this transformation is oligomeric azaindocane 3, [N(CH₂CH₂NSiMe₃)₂In(CH₂CH₂NSiMe₃)]₃. The composition and structures of new compounds have been established by ¹H and ¹³C NMR spectroscopy. The crystal structures of 1·Py, trans‐2, and 3 have been determined by X‐ray diffraction studies. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)

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Shutov P. L. et al. Reaction of [In(NEt2)3]2 with N(CH 2CH2NSiMe3H)3: Synthesis and characterization of new azaindatranes and azaindocane // European Journal of Inorganic Chemistry. 2004. Vol. 2004. No. 10. pp. 2123-2129.

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Shutov P. L., Karlov S. S., Harms K., Churakov A. V., Lorberth J., Zaitseva G. S. Reaction of [In(NEt2)3]2 with N(CH 2CH2NSiMe3H)3: Synthesis and characterization of new azaindatranes and azaindocane // European Journal of Inorganic Chemistry. 2004. Vol. 2004. No. 10. pp. 2123-2129.

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TY - JOUR

DO - 10.1002/ejic.200300875

UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.200300875

TI - Reaction of [In(NEt2)3]2 with N(CH 2CH2NSiMe3H)3: Synthesis and characterization of new azaindatranes and azaindocane

T2 - European Journal of Inorganic Chemistry

AU - Shutov, Pavel L

AU - Karlov, Sergey S.

AU - Harms, K.

AU - Churakov, Andrei V.

AU - Lorberth, Jörg

AU - Zaitseva, Galina S.

PY - 2004

DA - 2004/05/01

PB - Wiley

SP - 2123-2129

IS - 10

VL - 2004

SN - 1434-1948

SN - 1099-0682

ER -

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@article{2004_Shutov,

author = {Pavel L Shutov and Sergey S. Karlov and K. Harms and Andrei V. Churakov and Jörg Lorberth and Galina S. Zaitseva},

title = {Reaction of [In(NEt2)3]2 with N(CH 2CH2NSiMe3H)3: Synthesis and characterization of new azaindatranes and azaindocane},

journal = {European Journal of Inorganic Chemistry},

year = {2004},

volume = {2004},

publisher = {Wiley},

month = {may},

url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.200300875},

number = {10},

pages = {2123--2129},

doi = {10.1002/ejic.200300875}

}

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Shutov, Pavel L., et al. “Reaction of [In(NEt2)3]2 with N(CH 2CH2NSiMe3H)3: Synthesis and characterization of new azaindatranes and azaindocane.” European Journal of Inorganic Chemistry, vol. 2004, no. 10, May. 2004, pp. 2123-2129. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.200300875.