High-yielding synthesis of β-octaalkyl-meso-(bromophenyl)-substituted porphyrins and X-ray study of axial complexes of their zinc complexes with THF and 1,4-dioxane
Elena A. Mikhalitsyna
1
,
Sergey E. Nefedov
2
,
Sergey A. Syrbu
3
,
Aleksandr S. Semeikin
3
,
Oskar I. Koifman
3
,
3
ISCTU, prospekt F. Engelsa 7, Ivanovo 153000, Russian Federation
|
Publication type: Journal Article
Publication date: 2012-10-29
scimago Q2
wos Q3
SJR: 0.459
CiteScore: 3.9
Impact factor: 2.0
ISSN: 14341948, 10990682
Inorganic Chemistry
Abstract
New 5‐(4‐bromophenyl)‐3,7,12,13,17,18‐hexamethyl‐2,8‐dipentyl‐ and 5,15‐bis(4‐bromophenyl)‐2,8,12,18‐tetramethyl‐2,8,12,18‐tetrapentylporphyrins (H2P‐1 and H2P‐2) and their zinc metal complexes (ZnP‐1 and ZnP‐2, respectively) were synthesized in high yields by condensation of β‐tetraalkyl‐substituted dipyrromethanes with 2‐formyl‐3,4‐dialkylpyrroles or 4‐bromobenzaldehyde and subsequent metallation. X‐ray analysis data showed the formation of axial complexes of ZnP‐1 and ZnP‐2 with the solvent molecules of THF and dioxane in the solid state. Coordination of ZnP‐1 with dioxane led to polymer multidecker structures.
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Mikhalitsyna E. A. et al. High-yielding synthesis of β-octaalkyl-meso-(bromophenyl)-substituted porphyrins and X-ray study of axial complexes of their zinc complexes with THF and 1,4-dioxane // European Journal of Inorganic Chemistry. 2012. Vol. 2012. No. 36. pp. 5979-5990.
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Mikhalitsyna E. A., Tyurin V. S., Nefedov S. E., Syrbu S. A., Semeikin A. S., Koifman O. I., Beletskaya I. P. High-yielding synthesis of β-octaalkyl-meso-(bromophenyl)-substituted porphyrins and X-ray study of axial complexes of their zinc complexes with THF and 1,4-dioxane // European Journal of Inorganic Chemistry. 2012. Vol. 2012. No. 36. pp. 5979-5990.
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TY - JOUR
DO - 10.1002/ejic.201200868
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201200868
TI - High-yielding synthesis of β-octaalkyl-meso-(bromophenyl)-substituted porphyrins and X-ray study of axial complexes of their zinc complexes with THF and 1,4-dioxane
T2 - European Journal of Inorganic Chemistry
AU - Mikhalitsyna, Elena A.
AU - Tyurin, Vladimir S
AU - Nefedov, Sergey E.
AU - Syrbu, Sergey A.
AU - Semeikin, Aleksandr S.
AU - Koifman, Oskar I.
AU - Beletskaya, Irina P.
PY - 2012
DA - 2012/10/29
PB - Wiley
SP - 5979-5990
IS - 36
VL - 2012
SN - 1434-1948
SN - 1099-0682
ER -
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BibTex (up to 50 authors)
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@article{2012_Mikhalitsyna,
author = {Elena A. Mikhalitsyna and Vladimir S Tyurin and Sergey E. Nefedov and Sergey A. Syrbu and Aleksandr S. Semeikin and Oskar I. Koifman and Irina P. Beletskaya},
title = {High-yielding synthesis of β-octaalkyl-meso-(bromophenyl)-substituted porphyrins and X-ray study of axial complexes of their zinc complexes with THF and 1,4-dioxane},
journal = {European Journal of Inorganic Chemistry},
year = {2012},
volume = {2012},
publisher = {Wiley},
month = {oct},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201200868},
number = {36},
pages = {5979--5990},
doi = {10.1002/ejic.201200868}
}
Cite this
MLA
Copy
Mikhalitsyna, Elena A., et al. “High-yielding synthesis of β-octaalkyl-meso-(bromophenyl)-substituted porphyrins and X-ray study of axial complexes of their zinc complexes with THF and 1,4-dioxane.” European Journal of Inorganic Chemistry, vol. 2012, no. 36, Oct. 2012, pp. 5979-5990. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201200868.
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