Wiley
European Journal of Inorganic Chemistry
,  том 2017 ,  издание 29 ,  страницы 3561-3569

Mononuclear Dysprosium Thiocyanate Complexes with 2,2′-Bipyridine and 1,10-Phenanthroline: Synthesis, Crystal Structures, SIM Behavior, and Solid-Phase Transformations

Тип публикации: Journal Article
Дата публикации: 2017-08-10
Wiley
scimago Q2
wos Q3
БС2
SJR: 0.459
CiteScore: 3.9
Impact factor: 2.0
ISSN: 14341948, 10990682
Inorganic Chemistry
Краткое описание

Five new dysprosium complexes were synthesized and characterized: neutral Dy(NCS)3·6(H2O) (1), [Dy(NCS)3(H2O)(bpy)2]·0.5(bpy)·H2O (2), and [Dy(NCS)3(H2O)(phen)2]·phen·0.5H2O (3), as well as ionic [Hbpy][Dy(NCS)4(bpy)2]·H2O (4) and [Hphen][Dy(NCS)4(phen)2] (5). In all complexes, the metal coordination number (CN) is 8. All complexes exhibit single‐ion magnet behavior. The influence of the structural features on ΔE/kB values is discussed. The thermal behavior of the new compounds was studied under an inert atmosphere in the temperature range of 30–550 °C. The thermal stability of the complexes is determined by the presence of solvate molecules.

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Petrosyants S. P. et al. Mononuclear Dysprosium Thiocyanate Complexes with 2,2′-Bipyridine and 1,10-Phenanthroline: Synthesis, Crystal Structures, SIM Behavior, and Solid-Phase Transformations // European Journal of Inorganic Chemistry. 2017. Vol. 2017. No. 29. pp. 3561-3569.
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Petrosyants S. P., Dobrokhotova Z. V., Ilyukhin A. B., Efimov N. N., Gavrikov A., Gavrikov A. V., Vasilyev P., Vasilyev P. N., Novotortsev V. M. Mononuclear Dysprosium Thiocyanate Complexes with 2,2′-Bipyridine and 1,10-Phenanthroline: Synthesis, Crystal Structures, SIM Behavior, and Solid-Phase Transformations // European Journal of Inorganic Chemistry. 2017. Vol. 2017. No. 29. pp. 3561-3569.
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TY - JOUR
DO - 10.1002/ejic.201700537
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201700537
TI - Mononuclear Dysprosium Thiocyanate Complexes with 2,2′-Bipyridine and 1,10-Phenanthroline: Synthesis, Crystal Structures, SIM Behavior, and Solid-Phase Transformations
T2 - European Journal of Inorganic Chemistry
AU - Petrosyants, Svetlana P.
AU - Dobrokhotova, Zhanna V
AU - Ilyukhin, Andrey B.
AU - Efimov, Nikolay N.
AU - Gavrikov, A
AU - Gavrikov, Andrey V
AU - Vasilyev, Pavel
AU - Vasilyev, Pavel N
AU - Novotortsev, Vladimir M.
PY - 2017
DA - 2017/08/10
PB - Wiley
SP - 3561-3569
IS - 29
VL - 2017
SN - 1434-1948
SN - 1099-0682
ER -
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@article{2017_Petrosyants,
author = {Svetlana P. Petrosyants and Zhanna V Dobrokhotova and Andrey B. Ilyukhin and Nikolay N. Efimov and A Gavrikov and Andrey V Gavrikov and Pavel Vasilyev and Pavel N Vasilyev and Vladimir M. Novotortsev},
title = {Mononuclear Dysprosium Thiocyanate Complexes with 2,2′-Bipyridine and 1,10-Phenanthroline: Synthesis, Crystal Structures, SIM Behavior, and Solid-Phase Transformations},
journal = {European Journal of Inorganic Chemistry},
year = {2017},
volume = {2017},
publisher = {Wiley},
month = {aug},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201700537},
number = {29},
pages = {3561--3569},
doi = {10.1002/ejic.201700537}
}
MLA
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Petrosyants, Svetlana P., et al. “Mononuclear Dysprosium Thiocyanate Complexes with 2,2′-Bipyridine and 1,10-Phenanthroline: Synthesis, Crystal Structures, SIM Behavior, and Solid-Phase Transformations.” European Journal of Inorganic Chemistry, vol. 2017, no. 29, Aug. 2017, pp. 3561-3569. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201700537.