Synthesis of Cobalt-Iron Chalcogenide Clusters as Precursors for Catalysts of Oxygen Electroreduction in Alkali Media
Sergey S. Shapovalov
1, 2, 3, 4
,
I. V. Skabitsky
1, 3
,
Natalia A Mayorova
5, 6
,
Andrey A. Shiryaev
5, 6
,
A. A. Shiryaev
5, 6, 7, 8
,
V. A. Grinberg
5, 6
Publication type: Journal Article
Publication date: 2020-05-26
scimago Q2
wos Q3
SJR: 0.459
CiteScore: 3.9
Impact factor: 2.0
ISSN: 14341948, 10990682
Inorganic Chemistry
Abstract
New cobalt‐iron chalcogenide clusters C5HMe4Co(CO)E2Fe2(CO)6 (E = Se, Te) were prepared and characterized by IR and NMR spectroscopy; their structures were determined by single‐crystal XRD. Catalysts consisting of nanoparticles of bimetallic chalcogenides of cobalt and iron deposited on highly dispersed carbon black Vulcan XC‐72 were made from the synthesized clusters. Structural characteristics of these catalysts were assessed using X‐ray phase analysis (XRD), microprobe analysis (EDX), and transmission electron microscopy (TEM). It was shown that on the obtained catalysts oxygen electroreduction reaction in alkaline medium proceeds according to a four‐electron mechanism, and the catalysts are tolerant to methanol presence.
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Shapovalov S. S. et al. Synthesis of Cobalt-Iron Chalcogenide Clusters as Precursors for Catalysts of Oxygen Electroreduction in Alkali Media // European Journal of Inorganic Chemistry. 2020. Vol. 2020. No. 21. pp. 2055-2062.
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Shapovalov S. S., Skabitsky I. V., Mayorova N. A., Shiryaev A. A., Shiryaev A. A., Grinberg V. A. Synthesis of Cobalt-Iron Chalcogenide Clusters as Precursors for Catalysts of Oxygen Electroreduction in Alkali Media // European Journal of Inorganic Chemistry. 2020. Vol. 2020. No. 21. pp. 2055-2062.
Cite this
RIS
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TY - JOUR
DO - 10.1002/ejic.202000140
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.202000140
TI - Synthesis of Cobalt-Iron Chalcogenide Clusters as Precursors for Catalysts of Oxygen Electroreduction in Alkali Media
T2 - European Journal of Inorganic Chemistry
AU - Shapovalov, Sergey S.
AU - Skabitsky, I. V.
AU - Mayorova, Natalia A
AU - Shiryaev, Andrey A.
AU - Shiryaev, A. A.
AU - Grinberg, V. A.
PY - 2020
DA - 2020/05/26
PB - Wiley
SP - 2055-2062
IS - 21
VL - 2020
SN - 1434-1948
SN - 1099-0682
ER -
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BibTex (up to 50 authors)
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@article{2020_Shapovalov,
author = {Sergey S. Shapovalov and I. V. Skabitsky and Natalia A Mayorova and Andrey A. Shiryaev and A. A. Shiryaev and V. A. Grinberg},
title = {Synthesis of Cobalt-Iron Chalcogenide Clusters as Precursors for Catalysts of Oxygen Electroreduction in Alkali Media},
journal = {European Journal of Inorganic Chemistry},
year = {2020},
volume = {2020},
publisher = {Wiley},
month = {may},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.202000140},
number = {21},
pages = {2055--2062},
doi = {10.1002/ejic.202000140}
}
Cite this
MLA
Copy
Shapovalov, Sergey S., et al. “Synthesis of Cobalt-Iron Chalcogenide Clusters as Precursors for Catalysts of Oxygen Electroreduction in Alkali Media.” European Journal of Inorganic Chemistry, vol. 2020, no. 21, May. 2020, pp. 2055-2062. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.202000140.