Toward the Synthesis of Tetrazino-tetrazine 1,3,6,8-Tetraoxide (TTTO): An Approach to Non-annulated 1,2,3,4-Tetrazine 1,3-Dioxides
Тип публикации: Journal Article
Дата публикации: 2015-08-19
SCImago Q2
WOS Q2
БС2
SJR: 0.497
CiteScore: 4.2
Impact factor: 2.8
ISSN: 1434193X, 10990690
Organic Chemistry
Physical and Theoretical Chemistry
Краткое описание
A novel approach for the synthesis of 6-(tert-butyl-NNO-azoxy)-5-methylthio-1,2,3,4-tetrazine 1,3-dioxide (1) was developed. This compound is likely to be a precursor of tetrazino-tetrazine 1,3,6,8-tetraoxide. The synthetic strategy consists of four steps: a synthesis of bis(tert-butyl-NNO-azoxy)methane, coupling of the latter with dimethyl nitrodithioimidocarbonate to give N-nitroimine 3, O-alkylation of the latter to O-alkylated nitroenamine and its reaction with BF3·Et2O to afford tetrazine 1,3-dioxide 1. An X-ray diffraction study of 1 was accomplished.
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Klenov M. S. et al. Toward the Synthesis of Tetrazino-tetrazine 1,3,6,8-Tetraoxide (TTTO): An Approach to Non-annulated 1,2,3,4-Tetrazine 1,3-Dioxides // European Journal of Organic Chemistry. 2015. Vol. 2015. No. 28. pp. 6170-6179.
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Klenov M. S., Anikin O. V., Churakov A. M., Strelenko Y. A., Fedyanin I. V., Ananyev I. V., Tartakovsky V. A. Toward the Synthesis of Tetrazino-tetrazine 1,3,6,8-Tetraoxide (TTTO): An Approach to Non-annulated 1,2,3,4-Tetrazine 1,3-Dioxides // European Journal of Organic Chemistry. 2015. Vol. 2015. No. 28. pp. 6170-6179.
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TY - JOUR
DO - 10.1002/ejoc.201500923
UR - https://doi.org/10.1002/ejoc.201500923
TI - Toward the Synthesis of Tetrazino-tetrazine 1,3,6,8-Tetraoxide (TTTO): An Approach to Non-annulated 1,2,3,4-Tetrazine 1,3-Dioxides
T2 - European Journal of Organic Chemistry
AU - Klenov, Michael S
AU - Anikin, Oleg V
AU - Churakov, Aleksandr M
AU - Strelenko, Yurii A.
AU - Fedyanin, Ivan V.
AU - Ananyev, Ivan V
AU - Tartakovsky, Vladimir A
PY - 2015
DA - 2015/08/19
PB - Wiley
SP - 6170-6179
IS - 28
VL - 2015
SN - 1434-193X
SN - 1099-0690
ER -
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@article{2015_Klenov,
author = {Michael S Klenov and Oleg V Anikin and Aleksandr M Churakov and Yurii A. Strelenko and Ivan V. Fedyanin and Ivan V Ananyev and Vladimir A Tartakovsky},
title = {Toward the Synthesis of Tetrazino-tetrazine 1,3,6,8-Tetraoxide (TTTO): An Approach to Non-annulated 1,2,3,4-Tetrazine 1,3-Dioxides},
journal = {European Journal of Organic Chemistry},
year = {2015},
volume = {2015},
publisher = {Wiley},
month = {aug},
url = {https://doi.org/10.1002/ejoc.201500923},
number = {28},
pages = {6170--6179},
doi = {10.1002/ejoc.201500923}
}
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Klenov, Michael S., et al. “Toward the Synthesis of Tetrazino-tetrazine 1,3,6,8-Tetraoxide (TTTO): An Approach to Non-annulated 1,2,3,4-Tetrazine 1,3-Dioxides.” European Journal of Organic Chemistry, vol. 2015, no. 28, Aug. 2015, pp. 6170-6179. https://doi.org/10.1002/ejoc.201500923.
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