The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups
Publication type: Journal Article
Publication date: 2007-02-12
scimago Q2
wos Q3
SJR: 0.461
CiteScore: 3.9
Impact factor: 2.0
ISSN: 07213115, 15214087
General Chemistry
General Chemical Engineering
Abstract
N- and O-Trifluoroacetylation has been used to protect secondary amine groups and hydroxyl groups respectively under nitrolysis/nitration conditions. The trifluoroacetyl protecting group may be readily removed from the nitrated products by solvolysis under mild conditions. The energetic molecules that have been produced by this methodology include 2,6,8,12-tetranitro- and 2,4,6,8,12-pentanitro-2,4,6,8,10,12-hexaazaisowurtzitane, 2-hydroxymethyl-2-methyl-1,3-dinitratopropane [2,2-bis(nitratomethyl)-propan-1-ol] and N-nitroazetidin-3-ol.
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Bellamy A. J. et al. The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups // Propellants, Explosives, Pyrotechnics. 2007. Vol. 32. No. 1. pp. 20-31.
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Bellamy A. J., Maccuish A., Golding P., Mahon M. F. The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups // Propellants, Explosives, Pyrotechnics. 2007. Vol. 32. No. 1. pp. 20-31.
Cite this
RIS
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TY - JOUR
DO - 10.1002/prep.200700004
UR - https://doi.org/10.1002/prep.200700004
TI - The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups
T2 - Propellants, Explosives, Pyrotechnics
AU - Bellamy, Anthony J
AU - Maccuish, Alistair
AU - Golding, Peter
AU - Mahon, Mary F.
PY - 2007
DA - 2007/02/12
PB - Wiley
SP - 20-31
IS - 1
VL - 32
SN - 0721-3115
SN - 1521-4087
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2007_Bellamy,
author = {Anthony J Bellamy and Alistair Maccuish and Peter Golding and Mary F. Mahon},
title = {The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups},
journal = {Propellants, Explosives, Pyrotechnics},
year = {2007},
volume = {32},
publisher = {Wiley},
month = {feb},
url = {https://doi.org/10.1002/prep.200700004},
number = {1},
pages = {20--31},
doi = {10.1002/prep.200700004}
}
Cite this
MLA
Copy
Bellamy, Anthony J., et al. “The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups.” Propellants, Explosives, Pyrotechnics, vol. 32, no. 1, Feb. 2007, pp. 20-31. https://doi.org/10.1002/prep.200700004.