The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups
Тип публикации: Journal Article
Дата публикации: 2007-02-12
scimago Q2
wos Q3
БС2
SJR: 0.461
CiteScore: 3.9
Impact factor: 2
ISSN: 07213115, 15214087
General Chemistry
General Chemical Engineering
Краткое описание
N- and O-Trifluoroacetylation has been used to protect secondary amine groups and hydroxyl groups respectively under nitrolysis/nitration conditions. The trifluoroacetyl protecting group may be readily removed from the nitrated products by solvolysis under mild conditions. The energetic molecules that have been produced by this methodology include 2,6,8,12-tetranitro- and 2,4,6,8,12-pentanitro-2,4,6,8,10,12-hexaazaisowurtzitane, 2-hydroxymethyl-2-methyl-1,3-dinitratopropane [2,2-bis(nitratomethyl)-propan-1-ol] and N-nitroazetidin-3-ol.
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Bellamy A. J. et al. The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups // Propellants, Explosives, Pyrotechnics. 2007. Vol. 32. No. 1. pp. 20-31.
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Bellamy A. J., Maccuish A., Golding P., Mahon M. F. The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups // Propellants, Explosives, Pyrotechnics. 2007. Vol. 32. No. 1. pp. 20-31.
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TY - JOUR
DO - 10.1002/prep.200700004
UR - https://doi.org/10.1002/prep.200700004
TI - The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups
T2 - Propellants, Explosives, Pyrotechnics
AU - Bellamy, Anthony J
AU - Maccuish, Alistair
AU - Golding, Peter
AU - Mahon, Mary F.
PY - 2007
DA - 2007/02/12
PB - Wiley
SP - 20-31
IS - 1
VL - 32
SN - 0721-3115
SN - 1521-4087
ER -
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@article{2007_Bellamy,
author = {Anthony J Bellamy and Alistair Maccuish and Peter Golding and Mary F. Mahon},
title = {The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups},
journal = {Propellants, Explosives, Pyrotechnics},
year = {2007},
volume = {32},
publisher = {Wiley},
month = {feb},
url = {https://doi.org/10.1002/prep.200700004},
number = {1},
pages = {20--31},
doi = {10.1002/prep.200700004}
}
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MLA
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Bellamy, Anthony J., et al. “The Use of Trifluoroacetyl as an N- and O-Protecting Group during the Synthesis of Energetic Compounds containing Nitramine and/or Nitrate Ester Groups.” Propellants, Explosives, Pyrotechnics, vol. 32, no. 1, Feb. 2007, pp. 20-31. https://doi.org/10.1002/prep.200700004.