Propellants, Explosives, Pyrotechnics

, том 40 , издание 1 , страницы 39-45

Synthesis and Properties of Hydrogen‐Free Detonation Diamond

Тип публикации: Journal Article

Дата публикации: 2014-08-21

Wiley

Propellants, Explosives, Pyrotechnics

SCImago Q2

WOS Q3

БС2

SJR: 0.496

CiteScore: 3.9

Impact factor: 2

ISSN: 07213115, 15214087

DOI: 10.1002/prep.201400039

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General Chemistry

General Chemical Engineering

Краткое описание

Detonation-prepared nanocrystalline diamond powders usually contain hydrogen. Herein, the synthesis of practically hydrogen-free nanodiamond particles by detonation of benzotrifuroxan (BTF) and their comprehensive characterization by elemental analysis, X-ray diffraction, electron microscopy, DSC/TGA, and BTE specific-surface determination is described. The effects of the porosity of BTF and of various neutral or carbonic admixtures to the explosive on the reaction thermodynamics as well as the yield and properties of the product were explored theoretically and experimentally. Hydrogen contamination of nanodiamond was investigated using solid-state NMR spectroscopy and possible sources of hydrogen explored. Admixing hygroscopic solids to the explosive introduced 0.1 to 0.6 % of hydrogen, as did purification in acidic (rather than neutral) media.

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ГОСТ |

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Batsanov S. S. et al. Synthesis and Properties of Hydrogen‐Free Detonation Diamond // Propellants, Explosives, Pyrotechnics. 2014. Vol. 40. No. 1. pp. 39-45.

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Batsanov S. S., Osavchuk A. N., Naumov S. P., Efimov A. E., Mendis B. G., Apperley D. C., Batsanov A. S. Synthesis and Properties of Hydrogen‐Free Detonation Diamond // Propellants, Explosives, Pyrotechnics. 2014. Vol. 40. No. 1. pp. 39-45.

RIS |

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TY - JOUR

DO - 10.1002/prep.201400039

UR - https://doi.org/10.1002/prep.201400039

TI - Synthesis and Properties of Hydrogen‐Free Detonation Diamond

T2 - Propellants, Explosives, Pyrotechnics

AU - Batsanov, Stepan S.

AU - Osavchuk, Alexander N

AU - Naumov, Stepan P

AU - Efimov, Alexander E

AU - Mendis, Budhika G

AU - Apperley, David C.

AU - Batsanov, Andrei S.

PY - 2014

DA - 2014/08/21

PB - Wiley

SP - 39-45

IS - 1

VL - 40

SN - 0721-3115

SN - 1521-4087

ER -

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@article{2014_Batsanov,

author = {Stepan S. Batsanov and Alexander N Osavchuk and Stepan P Naumov and Alexander E Efimov and Budhika G Mendis and David C. Apperley and Andrei S. Batsanov},

title = {Synthesis and Properties of Hydrogen‐Free Detonation Diamond},

journal = {Propellants, Explosives, Pyrotechnics},

year = {2014},

volume = {40},

publisher = {Wiley},

month = {aug},

url = {https://doi.org/10.1002/prep.201400039},

number = {1},

pages = {39--45},

doi = {10.1002/prep.201400039}

}

MLA

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MLA Скопировать

Batsanov, Stepan S., et al. “Synthesis and Properties of Hydrogen‐Free Detonation Diamond.” Propellants, Explosives, Pyrotechnics, vol. 40, no. 1, Aug. 2014, pp. 39-45. https://doi.org/10.1002/prep.201400039.

Издатель

Wiley

Журнал

Propellants, Explosives, Pyrotechnics

SCImago Q2

WOS Q3

БС2

SJR

0.496

CiteScore

3.9

Impact factor

ISSN

07213115 (Print)

15214087 (Electronic)

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